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MS-NW-6678 3-indoleacetohydrazide C10H11N3O (Mass of molecular ion: 189)
Source Temperature: 200 °C Sample Temperature: 130 °C Direct, 75 eV
18.0 3.8 28.0 2.1 31.0 3.1 39.0 1.8 50.0 2.7 51.0 4.8 52.0 2.3 62.0 1.0 63.0 2.5 65.0 2.0 74.0 2.0 75.0 2.9 76.0 3.6 77.0 13.7 78.0 1.7 101.0 2.1 102.0 7.0 103.0 10.2 104.0 1.3 117.0 1.2 128.0 4.1 129.0 9.9 130.0 100.0 131.0 11.0 144.0 17.6 145.0 2.2 146.0 1.0 157.0 3.6 158.0 3.4 189.0 24.8 190.0 3.3
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C10 H11 N3 O 0.039 g : 0.5 ml DMSO-d6 3-indoleacetohydrazide Assign. Shift(ppm)
A 10.9 B 9.15 C 7.579 D 7.338 E 7.187 F 7.062 G 6.974 J 4.21 K 3.464
Hz ppm Int.
4343.61 10.869 146 3658.20 9.154 201 3033.42 7.591 217 3033.05 7.590 219 3025.54 7.571 237 3025.18 7.570 232 2937.07 7.350 272 2928.83 7.329 319 2873.52 7.191 316 2871.32 7.185 306 2831.02 7.084 117 2829.92 7.081 127 2824.06 7.067 191 2822.96 7.064 253 2821.86 7.061 134 2816.00 7.047 161 2814.72 7.043 150 2794.94 6.994 178 2794.20 6.992 176 2787.06 6.974 271 2786.33 6.972 198 2780.10 6.957 124 2779.00 6.954 114 1683.67 4.213 413 1384.56 3.465 1000
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