5,6-二氯-3-吡啶甲醇

产品名称 5,6-二氯-3-吡啶甲醇

CAS号54127-30-9

分子式C6H5Cl2NO

分子量178.02

¹³CNMR

Mass

MS-IW-8669          
(5,6-dichloro-3-pyridyl)methanol
C6H5Cl2NO           (Mass of molecular ion:    177)

   Source Temperature: 210 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      18.0       2.3
      26.0       1.5
      27.0       3.1
      28.0       7.4
      29.0       7.8
      31.0      12.9
      32.0       1.2
      36.0       2.9
      37.0       3.1
      38.0       3.8
      39.0       4.1
      41.0       1.1
      43.0       1.0
      47.0       1.5
      48.0       1.9
      49.0       5.2
      50.0      12.1
      51.0      17.2
      52.0       4.5
      53.0       2.5
      55.0       3.4
      56.5       1.0
      57.0       1.3
      60.0       2.5
      61.0       4.1
      62.0       5.7
      63.0       4.5
      64.0       1.8
      69.0       1.2
      70.5       2.5
      72.0       2.4
      73.0       5.4
      74.0       2.1
      75.0       6.9
      76.0      22.1
      77.0       3.0
      78.0      23.3
      79.0       3.2
      83.0       1.2
      84.0       5.8
      85.0      11.7
      86.0       5.1
      87.0      10.2
      88.0       3.7
      89.0       3.5
      90.0       1.2
      91.0       1.8
      92.0       1.1
      96.0       1.1
      97.0       4.6
      98.0       1.4
      99.0       2.7
     105.0       1.4
     106.0      15.1
     107.0       3.1
     109.0       2.1
     110.0       7.1
     111.0       2.5
     112.0      77.7
     113.0      12.8
     114.0      35.3
     115.0      11.4
     116.0       4.2
     117.0       2.4
     119.0       1.5
     121.0       2.3
     123.0       1.2
     124.0      12.9
     125.0       4.3
     126.0       4.8
     127.0       1.4
     133.0       3.2
     134.0       1.0
     135.0       2.6
     140.0       6.4
     141.0       3.4
     142.0      37.6
     143.0       3.7
     144.0      11.7
     146.0       6.0
     147.0       5.0
     148.0     100.0
     149.0       9.4
     150.0      62.6
     151.0       4.5
     152.0      10.1
     159.0       6.4
     160.0       9.5
     161.0       5.4
     162.0       6.2
     163.0       1.4
     164.0       1.2
     174.0       4.9
     175.0       2.5
     176.0      56.7
     177.0      87.2
     178.0      42.0
     179.0      55.7
     180.0      10.2
     181.0       9.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₆ H₅ Cl₂ N O	0.039 g : 0.5 ml CDCl₃
(5,6-dichloro-3-pyridyl)methanol

    Assign.     Shift(ppm)

      A             8.218
      B             7.835
      C             4.728
      D             3.38

     Hz     ppm     Int.

   3285.40   8.221    414
   3284.79   8.220    294
   3284.06   8.218    296
   3283.33   8.216    419
   3133.06   7.840    280
   3132.32   7.838    486
   3131.59   7.836    308
   3130.98   7.835    305
   3130.25   7.833    462
   3129.52   7.831    254
   1889.65   4.729   1000
   1351.56   3.382     44

in CDCl3

KBr disc

nujol mull

更多供应商

5,6-二氯-3-吡啶甲醇(54127-30-9)质谱(MS) 相关产品图谱

5,6-二氯烟酸(41667-95-2)核磁图(¹³CNMR) 5,6-二氯烟酸(41667-95-2)质谱(MS) 5,6-二氯烟酸(41667-95-2)核磁图(¹HNMR) 5,6-二氯烟酸(41667-95-2)红外图谱(IR2) 5,6-二氯烟酸(41667-95-2)红外图谱(IR1)

展开收起