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网站主页CAS数据库列表 538-51-2更多图谱N-苄叉苯胺(538-51-2)红外图谱(IR2)

N-苄叉苯胺

产品名称 N-苄叉苯胺

CAS号538-51-2

分子式C13H11N

分子量181.23

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  • Mass

    MS-NW-5563          
    N-benzylideneaniline
    C13H11N             (Mass of molecular ion:    181)
    

       Source Temperature: 250 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          27.0       1.7
          28.0       1.3
          38.0       1.1
          39.0       3.8
          50.0       4.4
          51.0      20.3
          52.0       3.0
          62.0       1.1
          63.0       3.2
          64.0       1.8
          74.0       1.3
          75.0       1.4
          76.0       4.9
          77.0      58.6
          77.5       1.1
          78.0      13.8
          89.0       4.0
          89.5       2.1
          90.0       3.3
          90.5       3.1
         103.0       1.1
         104.0      14.5
         105.0       1.3
         151.0       1.1
         152.0       3.2
         153.0       1.4
         179.0       1.5
         180.0      95.2
         181.0     100.0
         182.0      13.7
         183.0       1.0
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C13 H11 N 0.040 g : 0.5 ml CDCl3
    N-benzylideneaniline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.433 B 7.891 C 7.46 D 7.378 E 7.22 F 7.20

         Hz     ppm     Int.
    

       3370.36   8.434    886
       3159.55   7.906    341
       3157.35   7.901    396
       3153.93   7.892    351
       3153.20   7.890    348
       3151.98   7.887    207
       3150.63   7.884    223
       3149.54   7.881    359
       2987.06   7.475     99
       2986.45   7.473    102
       2985.23   7.470    148
       2983.03   7.465   1000
       2980.83   7.459    815
       2977.54   7.451    494
       2976.20   7.448    499
       2974.37   7.443    119
       2972.29   7.438    127
       2957.64   7.401    298
       2956.79   7.399    164
       2955.81   7.396    143
       2951.54   7.386    219
       2949.46   7.381    619
       2948.49   7.378    275
       2944.09   7.367    188
       2942.26   7.363    425
       2940.19   7.357     99
       2894.04   7.242    106
       2892.82   7.239    217
       2891.60   7.236    200
       2887.08   7.225    101
       2885.38   7.220    453
       2884.16   7.217    778
       2883.06   7.214    675
       2882.32   7.213    431
       2881.47   7.210    493
       2879.27   7.205    112
       2877.69   7.201    291
       2876.83   7.199    348
       2875.73   7.196    635
       2874.63   7.193    403
       2872.44   7.188     74
    


  • 1H NMR 89.56 MHz
    C13 H11 N 0.045 g : 0.5 ml CDCl3
    N-benzylideneaniline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.42 B 7.88 C 7.44 D 7.44 E 7.38 F 7.19 G 7.19

         Hz     ppm     Int.
    

        753.94   8.419    953
        711.06   7.940    252
        709.25   7.920    193
        708.56   7.912    252
        708.06   7.906    218
        706.75   7.892    234
        705.44   7.877    307
        704.31   7.865    266
        702.75   7.847    205
        701.50   7.833    390
        700.25   7.819    149
        697.81   7.792     86
        675.38   7.542     57
        672.94   7.514    119
        670.19   7.484    305
        669.25   7.473   1000
        668.00   7.459    460
        666.25   7.440    823
        665.38   7.430    375
        664.81   7.424    362
        664.31   7.418    368
        662.75   7.401    726
        661.19   7.383    292
        660.38   7.374    326
        660.00   7.370    335
        659.44   7.364    400
        657.63   7.343    124
        656.06   7.326    107
        654.50   7.308    686
        653.81   7.301    690
        651.88   7.279    198
        650.38   7.262    303
        649.56   7.253    570
        648.94   7.246    401
        647.94   7.235    716
        647.56   7.231    741
        647.06   7.225    744
        644.00   7.191    443
        641.88   7.168    189
        640.44   7.151    318
        639.81   7.144    284
        638.38   7.128    198
        636.50   7.107    101
        635.06   7.091     81
    

in CDCl3



KBr disc



nujol mull



4880 A,200 M,powder