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网站主页CAS数据库列表 5351-69-9更多图谱4-苯基-3-氨基硫脲(5351-69-9)Raman光谱

4-苯基-3-氨基硫脲

产品名称 4-苯基-3-氨基硫脲

CAS号5351-69-9

分子式C7H9N3S

分子量167.23

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  • Mass

    MS-NW-2083          
    4-phenyl(thiosemicarbazide)
    C7H9N3S             (Mass of molecular ion:    167)
    

       Source Temperature: 220 °C
       Sample Temperature: 140 °C
       Direct, 75 eV
    

          16.0       2.0
          17.0       3.7
          18.0       2.5
          27.0       2.1
          28.0       4.9
          29.0       1.4
          30.0       1.2
          31.0       4.1
          32.0     100.0
          33.0       1.5
          34.0       4.5
          37.0       1.6
          38.0       2.8
          39.0       8.1
          40.0       1.1
          41.0       1.0
          43.0       1.0
          45.0       2.3
          50.0       6.3
          51.0      21.2
          52.0       2.9
          59.0       1.1
          60.0       1.1
          62.0       1.2
          63.0       3.4
          64.0       3.5
          65.0      10.2
          66.0       6.1
          67.5       1.2
          74.0       3.0
          75.0       3.1
          76.0       3.3
          77.0      58.3
          78.0       6.6
          91.0       9.8
          92.0       5.1
          93.0      19.2
          94.0       1.7
         103.0       3.2
         104.0       4.5
         108.0       1.5
         109.0      11.2
         110.0       2.9
         118.0      14.4
         119.0       2.3
         133.0       4.1
         135.0      37.2
         136.0      28.6
         137.0       8.1
         138.0       1.6
         149.0       1.0
         150.0       1.9
         167.0      48.9
         168.0       4.8
         169.0       2.4
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C7 H9 N3 S 0.038 g : 0.5 ml DMSO-d6
    4-phenyl(thiosemicarbazide)
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 9.6 B *1 9.11 C 7.65 D 7.301 E 7.101 F 4.8

         Hz     ppm     Int.
    

       3642.12   9.114    419
       3080.14   7.708     23
       3078.31   7.703     27
       3060.00   7.657    343
       3057.71   7.651    329
       3053.89   7.642    371
       3036.80   7.599     31
       3036.04   7.597     29
       3035.28   7.595     26
       3034.06   7.592     24
       3033.14   7.590     23
       2925.72   7.321    613
       2923.74   7.316    274
       2918.09   7.302   1000
       2909.85   7.281    681
       2844.85   7.119    283
       2837.52   7.101    462
       2830.05   7.082    204
       1908.42   4.776     73
    

in CDCl3



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