4-苯基-3-氨基硫脲

Mass

MS-NW-2083          
4-phenyl(thiosemicarbazide)
C7H9N3S             (Mass of molecular ion:    167)

   Source Temperature: 220 °C
   Sample Temperature: 140 °C
   Direct, 75 eV

      16.0       2.0
      17.0       3.7
      18.0       2.5
      27.0       2.1
      28.0       4.9
      29.0       1.4
      30.0       1.2
      31.0       4.1
      32.0     100.0
      33.0       1.5
      34.0       4.5
      37.0       1.6
      38.0       2.8
      39.0       8.1
      40.0       1.1
      41.0       1.0
      43.0       1.0
      45.0       2.3
      50.0       6.3
      51.0      21.2
      52.0       2.9
      59.0       1.1
      60.0       1.1
      62.0       1.2
      63.0       3.4
      64.0       3.5
      65.0      10.2
      66.0       6.1
      67.5       1.2
      74.0       3.0
      75.0       3.1
      76.0       3.3
      77.0      58.3
      78.0       6.6
      91.0       9.8
      92.0       5.1
      93.0      19.2
      94.0       1.7
     103.0       3.2
     104.0       4.5
     108.0       1.5
     109.0      11.2
     110.0       2.9
     118.0      14.4
     119.0       2.3
     133.0       4.1
     135.0      37.2
     136.0      28.6
     137.0       8.1
     138.0       1.6
     149.0       1.0
     150.0       1.9
     167.0      48.9
     168.0       4.8
     169.0       2.4

Assign. Shift(ppm) A *1 9.6 B *1 9.11 C 7.65 D 7.301 E 7.101 F 4.8

     Hz     ppm     Int.

   3642.12   9.114    419
   3080.14   7.708     23
   3078.31   7.703     27
   3060.00   7.657    343
   3057.71   7.651    329
   3053.89   7.642    371
   3036.80   7.599     31
   3036.04   7.597     29
   3035.28   7.595     26
   3034.06   7.592     24
   3033.14   7.590     23
   2925.72   7.321    613
   2923.74   7.316    274
   2918.09   7.302   1000
   2909.85   7.281    681
   2844.85   7.119    283
   2837.52   7.101    462
   2830.05   7.082    204
   1908.42   4.776     73