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网站主页CAS数据库列表 53485-07-7更多图谱N-(3-氨丙基)-N-甲基苯胺(53485-07-7)核磁图(13CNMR)

N-(3-氨丙基)-N-甲基苯胺

产品名称 N-(3-氨丙基)-N-甲基苯胺

CAS号53485-07-7

分子式C10H16N2

分子量164.25

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  • Mass

    MS-IW-5791          
    N-methyl-n-phenyltrimethylenediamine
    C10H16N2            (Mass of molecular ion:    164)
    

       Source Temperature: 230 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          27.0       1.0
          28.0       2.3
          30.0       8.1
          39.0       2.1
          41.0       1.1
          42.0       6.5
          43.0       1.0
          44.0       2.6
          50.0       1.0
          51.0       4.8
          56.0       5.5
          57.0       6.3
          65.0       1.9
          70.0       1.3
          77.0      15.6
          78.0       2.7
          79.0       3.6
          91.0       5.4
          92.0       1.9
          93.0       1.8
         103.0       2.1
         104.0       8.3
         105.0       7.9
         106.0       9.0
         107.0      17.9
         108.0       6.1
         117.0       1.4
         118.0       3.6
         119.0       3.0
         120.0     100.0
         121.0      10.7
         132.0       6.3
         133.0       2.0
         134.0       3.6
         146.0       6.6
         147.0      14.1
         148.0       1.7
         164.0      22.8
         165.0       3.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10 H16 N2 0.05 ml : 0.5 ml CDCl3
    N-methyl-N-phenyltrimethylenediamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.205 B 6.69 C 6.67 D 3.342 E 2.887 F 2.701 G 1.681 J 1.25

         Hz     ppm     Int.
    

       2890.14   7.232     30
       2887.82   7.226    167
       2885.62   7.221     66
       2883.06   7.214     43
       2880.49   7.208    220
       2878.91   7.204    223
       2876.46   7.198     41
       2873.78   7.191     76
       2871.70   7.186    187
       2869.14   7.180     32
       2681.03   6.709    194
       2680.18   6.707    242
       2672.12   6.687    267
       2671.26   6.684    261
       2664.92   6.669    112
       2663.94   6.666    156
       2657.71   6.651     54
       2656.74   6.648     76
       1343.02   3.361    180
       1335.82   3.343    233
       1328.49   3.325    187
       1153.81   2.888   1000
       1147.71   2.872     31
       1086.67   2.720    203
       1079.83   2.702    320
       1072.75   2.685    214
        686.04   1.717     62
        678.83   1.699    158
        671.75   1.681    195
        664.55   1.663    150
        657.47   1.646     56
        501.34   1.255     74
    

in CDCl3



liquid film