N-乙基乙酰苯胺

产品名称 N-乙基乙酰苯胺

CAS号529-65-7

分子式C10H13NO

分子量163.22

¹³CNMR

Mass

MS-NW-7253          
N-ethylacetanilide
C10H13NO            (Mass of molecular ion:    163)

   Source Temperature: 210 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       1.1
      27.0       2.1
      28.0       1.1
      29.0       1.5
      39.0       3.0
      42.0       2.7
      43.0      19.9
      44.0       1.3
      50.0       1.7
      51.0       7.0
      52.0       1.3
      63.0       1.6
      64.0       1.6
      65.0       3.5
      66.0       1.3
      70.0       5.2
      77.0      16.7
      78.0       2.9
      79.0       2.7
      91.0       2.1
      92.0       1.9
      93.0       4.6
     104.0       4.1
     105.0       3.1
     106.0     100.0
     107.0       8.2
     118.0       1.8
     120.0       7.4
     121.0      15.1
     122.0       1.4
     135.0       6.1
     148.0       1.3
     163.0      22.5
     164.0       3.1

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₀ H₁₃ N O	0.048 g : 0.5 ml CDCl₃
N-ethylacetanilide

    Assign.     Shift(ppm)

      A          7.55 to 7.290
      B             7.18
      C             3.752
      D             1.826
      E             1.116

     Hz     ppm     Int.

    676.19   7.551     35
    674.19   7.528     30
    672.19   7.506     62
    670.50   7.487     55
    667.31   7.451    205
    666.25   7.440    151
    665.38   7.430    152
    664.25   7.417    154
    662.38   7.396    325
    661.50   7.387    403
    659.94   7.369    517
    656.88   7.335    181
    655.00   7.314    123
    654.63   7.310    120
    652.94   7.291     40
    652.00   7.281     48
    650.63   7.265     52
    649.13   7.248     66
    647.69   7.232     99
    645.88   7.212    423
    644.75   7.200    142
    643.19   7.182    229
    641.13   7.159    178
    640.06   7.147    135
    638.19   7.126    213
    636.19   7.104    198
    347.19   3.877    128
    340.00   3.797    402
    337.13   3.765     32
    332.88   3.717    425
    325.75   3.638    153
    169.88   1.897     31
    163.56   1.827    930
    156.81   1.751     37
    156.25   1.745     35
    106.88   1.194    491
    104.06   1.162     45
     99.81   1.115   1000
     96.38   1.077     50
     95.88   1.071     49
     95.44   1.066     50
     92.56   1.034    432

in CDCl3

KBr disc

nujol mull

4880 A,200 M,powder

更多供应商

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