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网站主页CAS数据库列表 529-65-7更多图谱N-乙基乙酰苯胺(529-65-7)核磁图(13CNMR)

N-乙基乙酰苯胺

产品名称 N-乙基乙酰苯胺

CAS号529-65-7

分子式C10H13NO

分子量163.22

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  • Mass

    MS-NW-7253          
    N-ethylacetanilide
    C10H13NO            (Mass of molecular ion:    163)
    

       Source Temperature: 210 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          15.0       1.1
          27.0       2.1
          28.0       1.1
          29.0       1.5
          39.0       3.0
          42.0       2.7
          43.0      19.9
          44.0       1.3
          50.0       1.7
          51.0       7.0
          52.0       1.3
          63.0       1.6
          64.0       1.6
          65.0       3.5
          66.0       1.3
          70.0       5.2
          77.0      16.7
          78.0       2.9
          79.0       2.7
          91.0       2.1
          92.0       1.9
          93.0       4.6
         104.0       4.1
         105.0       3.1
         106.0     100.0
         107.0       8.2
         118.0       1.8
         120.0       7.4
         121.0      15.1
         122.0       1.4
         135.0       6.1
         148.0       1.3
         163.0      22.5
         164.0       3.1
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C10 H13 N O 0.048 g : 0.5 ml CDCl3
    N-ethylacetanilide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.55 to 7.290 B 7.18 C 3.752 D 1.826 E 1.116

         Hz     ppm     Int.
    

        676.19   7.551     35
        674.19   7.528     30
        672.19   7.506     62
        670.50   7.487     55
        667.31   7.451    205
        666.25   7.440    151
        665.38   7.430    152
        664.25   7.417    154
        662.38   7.396    325
        661.50   7.387    403
        659.94   7.369    517
        656.88   7.335    181
        655.00   7.314    123
        654.63   7.310    120
        652.94   7.291     40
        652.00   7.281     48
        650.63   7.265     52
        649.13   7.248     66
        647.69   7.232     99
        645.88   7.212    423
        644.75   7.200    142
        643.19   7.182    229
        641.13   7.159    178
        640.06   7.147    135
        638.19   7.126    213
        636.19   7.104    198
        347.19   3.877    128
        340.00   3.797    402
        337.13   3.765     32
        332.88   3.717    425
        325.75   3.638    153
        169.88   1.897     31
        163.56   1.827    930
        156.81   1.751     37
        156.25   1.745     35
        106.88   1.194    491
        104.06   1.162     45
         99.81   1.115   1000
         96.38   1.077     50
         95.88   1.071     49
         95.44   1.066     50
         92.56   1.034    432
    

in CDCl3



KBr disc



nujol mull



4880 A,200 M,powder