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MassMS-NW-7207 3-nitrosalicylaldehyde C7H5NO4 (Mass of molecular ion: 167)
Source Temperature: 220 °C Sample Temperature: 190 °C Reservoir, 75 eV
18.0 1.1 26.0 1.3 27.0 3.1 28.0 4.3 29.0 5.1 30.0 4.3 37.0 4.7 38.0 9.0 39.0 25.1 40.0 1.2 49.0 1.6 50.0 5.7 51.0 8.1 52.0 3.0 53.0 10.9 55.0 2.2 61.0 3.4 62.0 8.3 63.0 27.7 64.0 14.3 65.0 19.2 66.0 3.4 67.0 1.0 74.0 3.2 75.0 4.4 76.0 1.7 77.0 5.6 78.0 2.2 79.0 1.0 81.0 1.8 91.0 35.9 92.0 26.0 93.0 6.0 105.0 1.5 107.0 1.2 119.0 27.2 120.0 42.4 121.0 9.1 149.0 100.0 150.0 11.3 151.0 1.5 166.0 4.6 167.0 17.2 168.0 1.6
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H5 N O4 0.051 g : 0.5 ml CDCl3 3-nitrosalicylaldehyde 
Assign. Shift(ppm)
A 11.45 B 10.401 C 8.345 D 8.111 E 7.163 J(B,E)=0.5HZ.
Hz ppm Int.1025.32 11.449 997 931.79 10.405 1000 931.27 10.399 865 752.86 8.407 290 751.03 8.386 324 744.51 8.313 329 742.75 8.294 384 731.40 8.167 265 729.57 8.147 243 723.78 8.082 328 721.95 8.062 275 649.00 7.247 269 648.49 7.241 249 640.80 7.155 418 633.03 7.069 199 632.52 7.063 183
in CDCl3
KBr disc
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