3-硝基水杨醛

Mass

MS-NW-7207          
3-nitrosalicylaldehyde
C7H5NO4             (Mass of molecular ion:    167)

   Source Temperature: 220 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      18.0       1.1
      26.0       1.3
      27.0       3.1
      28.0       4.3
      29.0       5.1
      30.0       4.3
      37.0       4.7
      38.0       9.0
      39.0      25.1
      40.0       1.2
      49.0       1.6
      50.0       5.7
      51.0       8.1
      52.0       3.0
      53.0      10.9
      55.0       2.2
      61.0       3.4
      62.0       8.3
      63.0      27.7
      64.0      14.3
      65.0      19.2
      66.0       3.4
      67.0       1.0
      74.0       3.2
      75.0       4.4
      76.0       1.7
      77.0       5.6
      78.0       2.2
      79.0       1.0
      81.0       1.8
      91.0      35.9
      92.0      26.0
      93.0       6.0
     105.0       1.5
     107.0       1.2
     119.0      27.2
     120.0      42.4
     121.0       9.1
     149.0     100.0
     150.0      11.3
     151.0       1.5
     166.0       4.6
     167.0      17.2
     168.0       1.6

Assign. Shift(ppm) A 11.45 B 10.401 C 8.345 D 8.111 E 7.163 J(B,E)=0.5HZ.

     Hz     ppm     Int.

   1025.32  11.449    997
    931.79  10.405   1000
    931.27  10.399    865
    752.86   8.407    290
    751.03   8.386    324
    744.51   8.313    329
    742.75   8.294    384
    731.40   8.167    265
    729.57   8.147    243
    723.78   8.082    328
    721.95   8.062    275
    649.00   7.247    269
    648.49   7.241    249
    640.80   7.155    418
    633.03   7.069    199
    632.52   7.063    183