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网站主页CAS数据库列表 51800-99-8更多图谱3-七氟丁酰-D-樟脑(51800-99-8)红外图谱(IR1)

3-七氟丁酰-D-樟脑

产品名称 3-七氟丁酰-D-樟脑

CAS号51800-99-8

分子式C14H15F7O2

分子量348.26


  • Mass

    MS-NW-7728          
    3-heptafluorobutyryl-(+)-camphor
    C14H15F7O2          (Mass of molecular ion:    348)
    

       Source Temperature: 130 °C
       Sample Temperature: 100 °C
       Direct, 75 eV
    

          18.0       3.2
          27.0      10.2
          28.0       1.9
          29.0       8.8
          31.0       1.0
          39.0      16.0
          40.0       3.3
          41.0      42.1
          42.0       2.6
          43.0      23.4
          45.0       3.3
          50.0       1.3
          51.0       4.5
          52.0       2.3
          53.0      10.3
          54.0       2.7
          55.0      28.8
          56.0       2.4
          57.0       5.3
          59.0       2.5
          63.0       1.6
          65.0       5.4
          66.0       2.4
          67.0      13.3
          68.0       3.9
          69.0      14.8
          70.0       3.1
          71.0       1.3
          75.0       1.4
          77.0       9.3
          78.0       3.0
          79.0       9.4
          80.0       4.3
          81.0      10.0
          82.0       4.1
          83.0      20.2
          84.0       5.4
          90.0       1.1
          91.0      12.6
          92.0       2.0
          93.0       7.3
          94.0       2.7
          95.0      31.2
          96.0       3.7
          97.0       2.3
         100.0       2.2
         103.0       1.1
         105.0       4.1
         106.0       1.2
         107.0       8.0
         108.0      20.2
         109.0      11.8
         110.0       2.8
         115.0       1.0
         117.0       1.6
         118.0       1.0
         119.0      22.2
         120.0       2.3
         121.0       4.7
         122.0       4.7
         123.0      26.3
         124.0       3.1
         131.0       1.2
         133.0      10.4
         134.0       1.4
         135.0       9.4
         136.0       7.8
         137.0       5.1
         139.0       1.1
         145.0       1.0
         146.0       1.0
         149.0       1.8
         150.0       1.7
         151.0      50.7
         152.0       6.4
         153.0       1.0
         159.0       1.0
         161.0       3.0
         164.0       1.3
         169.0       5.0
         179.0      12.9
         180.0       1.5
         181.0       1.8
         201.0       1.3
         209.0       1.0
         249.0       1.0
         251.0       1.1
         259.0       1.1
         263.0       1.5
         264.0       1.2
         265.0       5.1
         273.0       1.2
         277.0       4.0
         278.0       1.3
         279.0       1.2
         285.0       2.1
         287.0       2.4
         291.0       4.1
         292.0       1.2
         293.0       1.1
         300.0       4.7
         301.0       5.2
         302.0       2.4
         304.0       1.8
         305.0      27.1
         306.0       9.1
         307.0       1.4
         315.0       2.6
         319.0       1.7
         320.0      43.1
         321.0       6.3
         329.0       1.0
         333.0      26.6
         334.0       3.9
         348.0     100.0
         349.0      16.3
         350.0       1.7
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C14 H15 F7 O2 0.05 ml : 0.5 ml CDCl3
    3-heptafluorobutyryl-(+)-camphor
    ChemicalStructure
        Assign.     Shift(ppm)
    A 12. B 2.870 C 2.09 D 1.78 E 1.48 F 1.45 G 1.020 J 0.976 K 0.832 ASSIGNED BY C-H COSY.

         Hz     ppm     Int.
    

       1147.27   2.871     70
       1146.84   2.870     70
       1141.50   2.857     39
        840.85   2.104     49
        837.00   2.095     65
        832.94   2.085     30
        829.52   2.076     30
        825.46   2.066     50
        730.37   1.828     42
        727.17   1.820     45
        717.55   1.796     55
        715.84   1.792     49
        714.35   1.788     61
        706.23   1.768     44
        607.72   1.521     32
        598.53   1.498     62
        594.68   1.489     86
        588.06   1.472    115
        585.92   1.467    141
        580.37   1.453     73
        577.16   1.445     59
        408.14   1.022   1000
        390.40   0.977    827
        385.49   0.965     41
        332.92   0.834    744
    

in CDCl3



liquid film



4880 A,200 M,liquid