图谱信息 供应商 相关产品
网站主页CAS数据库列表 5162-03-8更多图谱2-氯二苯甲酮(5162-03-8)质谱(MS)

2-氯二苯甲酮

产品名称 2-氯二苯甲酮

CAS号5162-03-8

分子式C13H9ClO

分子量216.66

展开


  • Mass

    MS-NW-7091          
    2-chlorobenzophenone
    C13H9ClO            (Mass of molecular ion:    216)
    

       Source Temperature: 270 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          18.0       3.8
          27.0       1.2
          28.0       3.0
          39.0       1.3
          50.0       7.2
          51.0      15.8
          52.0       1.0
          63.0       1.4
          74.0       3.4
          75.0      11.3
          76.0       7.5
          77.0      39.4
          78.0       2.9
          85.0       1.2
          94.0       1.3
         105.0     100.0
         106.0       7.7
         111.0      14.5
         112.0       1.3
         113.0       5.2
         139.0      42.1
         140.0       3.5
         141.0      14.0
         142.0       1.3
         150.0       1.0
         151.0       2.0
         152.0       4.4
         153.0       1.5
         180.0       1.3
         181.0       4.4
         188.0       1.0
         216.0      37.0
         217.0       5.7
         218.0      13.0
         219.0       1.9
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C13 H9 Cl O 0.040 g : 0.5 ml CDCl3
    2-chlorobenzophenone
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.816 B 7.594 C 7.461 D 7.46 E 7.43 F 7.37 G 7.36 CONFIRMED BY LAOCN CALCULATION

         Hz     ppm     Int.
    

       3129.88   7.832    106
       3128.17   7.828    544
       3127.69   7.827    449
       3126.95   7.825    663
       3121.83   7.812    218
       3119.87   7.807    749
       3118.53   7.804    693
       3044.92   7.619    102
       3043.70   7.616    186
       3042.36   7.613    106
       3038.09   7.602    140
       3036.25   7.598    416
       3034.55   7.594    145
       3030.15   7.583    182
       3028.81   7.579    309
       3027.59   7.576    163
       2991.58   7.486    139
       2989.99   7.482    526
       2988.40   7.478    255
       2986.57   7.473    222
       2985.35   7.470    195
       2982.42   7.463    699
       2982.06   7.462    725
       2980.71   7.459    327
       2979.86   7.457    519
       2978.88   7.454    564
       2978.03   7.452    801
       2977.42   7.451    580
       2976.32   7.448    265
       2974.61   7.444    695
       2972.90   7.439    426
       2969.60   7.431    464
       2966.92   7.424     80
       2964.60   7.418    125
       2961.55   7.411    200
       2956.54   7.398     44
       2952.88   7.389    113
       2952.03   7.387    140
       2948.49   7.378   1000
       2947.39   7.375    745
       2947.02   7.375    695
       2945.31   7.370    443
       2944.58   7.368    423
       2943.24   7.365    385
       2941.53   7.361    324
       2939.45   7.356     38
       2935.67   7.346     49
       2933.96   7.342     55
    

in CDCl3



KBr disc



nujol mull



4880 A,200 M,powder