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MS-NW-7091 2-chlorobenzophenone C13H9ClO (Mass of molecular ion: 216)
Source Temperature: 270 °C Sample Temperature: 190 °C Reservoir, 75 eV
18.0 3.8 27.0 1.2 28.0 3.0 39.0 1.3 50.0 7.2 51.0 15.8 52.0 1.0 63.0 1.4 74.0 3.4 75.0 11.3 76.0 7.5 77.0 39.4 78.0 2.9 85.0 1.2 94.0 1.3 105.0 100.0 106.0 7.7 111.0 14.5 112.0 1.3 113.0 5.2 139.0 42.1 140.0 3.5 141.0 14.0 142.0 1.3 150.0 1.0 151.0 2.0 152.0 4.4 153.0 1.5 180.0 1.3 181.0 4.4 188.0 1.0 216.0 37.0 217.0 5.7 218.0 13.0 219.0 1.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C13 H9 Cl O 0.040 g : 0.5 ml CDCl3 2-chlorobenzophenone Assign. Shift(ppm)
A 7.816 B 7.594 C 7.461 D 7.46 E 7.43 F 7.37 G 7.36 CONFIRMED BY LAOCN CALCULATION
Hz ppm Int.
3129.88 7.832 106 3128.17 7.828 544 3127.69 7.827 449 3126.95 7.825 663 3121.83 7.812 218 3119.87 7.807 749 3118.53 7.804 693 3044.92 7.619 102 3043.70 7.616 186 3042.36 7.613 106 3038.09 7.602 140 3036.25 7.598 416 3034.55 7.594 145 3030.15 7.583 182 3028.81 7.579 309 3027.59 7.576 163 2991.58 7.486 139 2989.99 7.482 526 2988.40 7.478 255 2986.57 7.473 222 2985.35 7.470 195 2982.42 7.463 699 2982.06 7.462 725 2980.71 7.459 327 2979.86 7.457 519 2978.88 7.454 564 2978.03 7.452 801 2977.42 7.451 580 2976.32 7.448 265 2974.61 7.444 695 2972.90 7.439 426 2969.60 7.431 464 2966.92 7.424 80 2964.60 7.418 125 2961.55 7.411 200 2956.54 7.398 44 2952.88 7.389 113 2952.03 7.387 140 2948.49 7.378 1000 2947.39 7.375 745 2947.02 7.375 695 2945.31 7.370 443 2944.58 7.368 423 2943.24 7.365 385 2941.53 7.361 324 2939.45 7.356 38 2935.67 7.346 49 2933.96 7.342 55
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