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MassMS-NW-9395 (+-)-6-phenyl-2,3,5,6-tetrahydroimidazo(2,1-b)thiazole hydrochloride C11H12N2S HCl (Mass of molecular ion: 204)
Source Temperature: 220 °C Sample Temperature: 140 °C Direct, 75 eV
15.0 1.1 18.0 2.7 27.0 3.8 28.0 6.6 29.0 1.6 30.0 1.4 35.0 3.2 36.0 33.1 37.0 1.1 38.0 10.7 39.0 4.7 41.0 2.6 42.0 3.1 45.0 8.8 46.0 1.1 50.0 2.8 51.0 7.5 52.0 1.8 54.0 3.2 55.0 1.3 56.0 7.9 59.0 2.4 60.0 2.6 61.0 1.2 62.0 1.3 63.0 4.6 64.0 1.6 65.0 3.0 69.0 1.9 71.0 1.1 72.0 5.1 73.0 60.8 74.0 3.6 75.0 3.8 76.0 2.3 77.0 12.3 78.0 3.9 88.0 1.9 89.0 7.7 90.0 3.8 91.0 6.3 98.0 2.0 99.0 3.2 100.0 1.5 101.0 59.6 102.0 6.6 103.0 9.6 104.0 15.3 105.0 1.7 115.0 1.1 116.0 3.2 117.0 6.5 118.0 2.4 121.0 13.1 122.0 2.3 126.0 2.9 127.0 18.9 128.0 2.2 129.0 1.3 130.0 1.4 131.0 2.0 143.0 1.1 144.0 1.9 148.0 87.2 149.0 10.3 150.0 4.6 175.0 1.3 176.0 5.9 177.0 1.0 202.0 2.6 203.0 34.2 204.0 100.0 205.0 15.8 206.0 5.5
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C11 H12 N2 S 0.038 g : 0.5 ml DMSO-d6 (+-)-6-phenyl-2,3,5,6-tetrahydroimidazo(2,1-b)thiazole hydrochloride 
Assign. Shift(ppm)
A 11.8 B 7.46 C 7.41 D 5.778 E *1 4.253 F 3.982 G *2 3.80 J *2 3.77 K *1 3.657
Hz ppm Int.2989.28 7.480 33 2987.63 7.476 78 2986.35 7.473 72 2982.32 7.463 1000 2979.39 7.455 700 2976.82 7.449 619 2974.26 7.443 84 2971.33 7.435 92 2969.68 7.431 133 2968.76 7.429 132 2967.30 7.425 61 2966.75 7.424 59 2964.73 7.419 145 2961.80 7.411 150 2959.97 7.407 103 2958.14 7.402 101 2955.94 7.397 136 2954.11 7.392 53 2952.46 7.388 64 2951.18 7.385 47 2949.90 7.382 42 2947.52 7.376 32 2318.89 5.803 154 2310.65 5.782 197 2308.63 5.777 188 2300.20 5.756 163 1710.23 4.280 182 1699.97 4.254 393 1689.71 4.228 188 1600.33 4.005 201 1592.63 3.986 507 1589.34 3.977 39 1585.49 3.968 371 1531.82 3.833 50 1524.86 3.816 91 1521.75 3.808 166 1519.73 3.803 32 1514.97 3.791 340 1511.86 3.783 32 1508.01 3.774 314 1500.13 3.754 124 1498.49 3.750 82 1490.24 3.729 34 1471.01 3.681 203 1462.58 3.660 220 1460.75 3.656 205 1452.51 3.635 190
in DMSO-d6
KBr disc
nujol mull
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