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网站主页CAS数据库列表 5086-74-8更多图谱盐酸四咪唑(5086-74-8)核磁图(13CNMR)

盐酸四咪唑

产品名称 盐酸四咪唑

CAS号5086-74-8

分子式C11H13ClN2S

分子量240.75

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  • Mass

    MS-NW-9395          
    (+-)-6-phenyl-2,3,5,6-tetrahydroimidazo(2,1-b)thiazole hydrochloride
    C11H12N2S HCl       (Mass of molecular ion:    204)
    

       Source Temperature: 220 °C
       Sample Temperature: 140 °C
       Direct, 75 eV
    

          15.0       1.1
          18.0       2.7
          27.0       3.8
          28.0       6.6
          29.0       1.6
          30.0       1.4
          35.0       3.2
          36.0      33.1
          37.0       1.1
          38.0      10.7
          39.0       4.7
          41.0       2.6
          42.0       3.1
          45.0       8.8
          46.0       1.1
          50.0       2.8
          51.0       7.5
          52.0       1.8
          54.0       3.2
          55.0       1.3
          56.0       7.9
          59.0       2.4
          60.0       2.6
          61.0       1.2
          62.0       1.3
          63.0       4.6
          64.0       1.6
          65.0       3.0
          69.0       1.9
          71.0       1.1
          72.0       5.1
          73.0      60.8
          74.0       3.6
          75.0       3.8
          76.0       2.3
          77.0      12.3
          78.0       3.9
          88.0       1.9
          89.0       7.7
          90.0       3.8
          91.0       6.3
          98.0       2.0
          99.0       3.2
         100.0       1.5
         101.0      59.6
         102.0       6.6
         103.0       9.6
         104.0      15.3
         105.0       1.7
         115.0       1.1
         116.0       3.2
         117.0       6.5
         118.0       2.4
         121.0      13.1
         122.0       2.3
         126.0       2.9
         127.0      18.9
         128.0       2.2
         129.0       1.3
         130.0       1.4
         131.0       2.0
         143.0       1.1
         144.0       1.9
         148.0      87.2
         149.0      10.3
         150.0       4.6
         175.0       1.3
         176.0       5.9
         177.0       1.0
         202.0       2.6
         203.0      34.2
         204.0     100.0
         205.0      15.8
         206.0       5.5
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C11 H12 N2 S 0.038 g : 0.5 ml DMSO-d6
    (+-)-6-phenyl-2,3,5,6-tetrahydroimidazo(2,1-b)thiazole hydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 11.8 B 7.46 C 7.41 D 5.778 E *1 4.253 F 3.982 G *2 3.80 J *2 3.77 K *1 3.657

         Hz     ppm     Int.
    

       2989.28   7.480     33
       2987.63   7.476     78
       2986.35   7.473     72
       2982.32   7.463   1000
       2979.39   7.455    700
       2976.82   7.449    619
       2974.26   7.443     84
       2971.33   7.435     92
       2969.68   7.431    133
       2968.76   7.429    132
       2967.30   7.425     61
       2966.75   7.424     59
       2964.73   7.419    145
       2961.80   7.411    150
       2959.97   7.407    103
       2958.14   7.402    101
       2955.94   7.397    136
       2954.11   7.392     53
       2952.46   7.388     64
       2951.18   7.385     47
       2949.90   7.382     42
       2947.52   7.376     32
       2318.89   5.803    154
       2310.65   5.782    197
       2308.63   5.777    188
       2300.20   5.756    163
       1710.23   4.280    182
       1699.97   4.254    393
       1689.71   4.228    188
       1600.33   4.005    201
       1592.63   3.986    507
       1589.34   3.977     39
       1585.49   3.968    371
       1531.82   3.833     50
       1524.86   3.816     91
       1521.75   3.808    166
       1519.73   3.803     32
       1514.97   3.791    340
       1511.86   3.783     32
       1508.01   3.774    314
       1500.13   3.754    124
       1498.49   3.750     82
       1490.24   3.729     34
       1471.01   3.681    203
       1462.58   3.660    220
       1460.75   3.656    205
       1452.51   3.635    190
    

in DMSO-d6



KBr disc



nujol mull