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MS-NW-7345 tetraphenylarsonium chloride C24H20AsCl H2O (Mass of molecular ion: 418)
Source Temperature: 200 °C Sample Temperature: 230 °C Direct, 75 eV
18.0 1.4 36.0 3.3 38.0 1.1 39.0 1.7 50.0 2.6 51.0 6.8 52.0 1.4 63.0 1.0 74.0 1.1 75.0 1.1 76.0 1.2 77.0 7.2 78.0 7.7 100.0 1.0 101.0 1.5 102.0 1.0 112.0 3.3 114.0 1.1 115.0 1.9 125.0 1.4 126.0 1.1 128.0 1.9 151.0 12.5 152.0 100.0 153.0 9.5 154.0 14.3 155.0 1.9 214.0 1.0 227.0 30.4 228.0 6.4 229.0 8.2 230.0 2.9 306.0 37.8 307.0 7.8 382.0 1.9 383.0 4.2 384.0 1.1
400 MHz in D2O
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1H NMR 399.65 MHz C24 H20 As Cl 0.042 g : 0.5 ml D2O tetraphenylarsonium chloride Assign. Shift(ppm)
A 7.944 B 7.784 C 7.729
Hz ppm Int.
3184.20 7.968 127 3182.83 7.965 236 3181.61 7.961 151 3179.17 7.955 48 3177.19 7.950 171 3175.35 7.946 504 3173.68 7.942 224 3169.40 7.931 205 3168.03 7.928 372 3166.66 7.924 220 3125.46 7.821 32 3123.63 7.816 43 3119.51 7.806 476 3117.83 7.802 262 3111.42 7.786 1000 3105.77 7.772 232 3103.64 7.766 788 3099.37 7.756 61 3098.91 7.755 59 3092.04 7.737 850 3091.13 7.735 982 3085.78 7.722 197 3083.95 7.717 544 3082.58 7.714 429
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