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MassMS-NW-1785 D-glucitol C6H14O6 (Mass of molecular ion: 182)
Source Temperature: 220 °C Sample Temperature: 180 °C Direct, 75 eV
14.0 1.0 15.0 15.7 17.0 1.4 18.0 6.9 19.0 18.0 26.0 1.5 27.0 10.7 28.0 13.8 29.0 18.4 30.0 3.2 31.0 34.8 32.0 2.0 39.0 3.6 41.0 8.0 42.0 9.3 43.0 48.6 44.0 32.0 45.0 32.0 46.0 1.6 47.0 2.0 55.0 11.5 56.0 31.6 57.0 25.3 58.0 1.8 59.0 1.8 60.0 18.1 61.0 83.7 62.0 3.2 69.0 4.5 71.0 7.1 72.0 1.7 73.0 100.0 74.0 46.2 75.0 3.5 85.0 10.9 86.0 1.9 87.0 1.6 89.0 1.1 91.0 7.8 97.0 2.0 103.0 41.5 104.0 4.6 115.0 4.0 133.0 12.3 146.0 1.0
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C6 H14 O6 0.040 g : 0.5 ml DMSO-d6 D-glucitol 
Assign. Shift(ppm)
A 4.56 B 4.49 C 4.48 D 4.39 E 4.34 F 4.12 G 3.671 J *1 3.58 K 3.55 L 3.48 M *2 3.44 N 3.39 P *1 3.37 Q *2 3.35 ASSIGNED BY H-H AND C-H COSY. J(A,K)=4.6HZ J(B,M)=J(B,Q)=6.2HZ J(C,L)=5.7HZ J(D,N)=5.9HZ J(E,J)=J(E,P)=5.7HZ J(F,G)=6.7HZ J(G,K)=4.4HZ J(G,N)=1.8HZ J(J,L)=3.3HZ J(K,M)=5.6HZ J(K,Q)=5.7HZ J(L,N)=7.8HZ J(L,P)=5.5HZ J(M,Q)=-11.0HZ
Hz ppm Int.1826.17 4.570 677 1821.53 4.558 690 1798.83 4.502 292 1792.60 4.486 1000 1786.87 4.472 855 1758.18 4.400 624 1752.32 4.385 646 1738.77 4.351 285 1733.03 4.337 654 1727.42 4.323 289 1650.39 4.130 673 1643.68 4.113 723 1473.88 3.688 156 1472.05 3.684 167 1469.48 3.677 201 1467.41 3.672 295 1465.33 3.667 176 1462.89 3.661 185 1460.94 3.656 181 1439.82 3.603 126 1436.52 3.595 145 1434.08 3.589 135 1430.66 3.580 172 1428.83 3.576 214 1425.54 3.567 216 1423.22 3.562 339 1419.68 3.553 284 1418.46 3.550 298 1412.96 3.536 213 1408.08 3.524 98 1403.56 3.512 72 1400.27 3.504 63 1397.71 3.498 142 1393.68 3.488 230 1392.21 3.484 188 1389.65 3.478 250 1387.82 3.473 266 1382.69 3.460 336 1380.86 3.456 159 1377.08 3.446 272 1371.70 3.433 168 1364.62 3.415 314 1363.65 3.413 268 1361.57 3.407 239 1359.62 3.403 248 1357.67 3.398 253 1355.59 3.392 361 1353.76 3.388 415 1348.51 3.375 477 1343.02 3.361 497 1337.40 3.347 369 1332.28 3.334 189 1326.54 3.320 114
in D2O
in DMSO-d6
KBr disc
nujol mull
4880 A,200 M,powder
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