1-氯蒽

Mass

MS-NW-7174          
1-chloroanthracene
C14H9Cl             (Mass of molecular ion:    212)

   Source Temperature: 210 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      50.0       1.2
      51.0       1.3
      62.0       1.8
      63.0       1.6
      74.0       2.6
      75.0       6.6
      75.5       1.8
      76.0       1.7
      86.0       1.1
      87.0       4.6
      87.5       2.7
      88.0      16.8
      88.5       4.0
      93.0       4.4
      94.0       1.5
      98.0       1.4
      99.0       1.4
     106.0      14.7
     106.5       2.6
     107.0       4.7
     126.0       1.3
     149.0       1.4
     150.0       5.2
     151.0       6.8
     152.0       1.2
     174.0       3.6
     175.0       5.0
     176.0      24.3
     177.0      11.3
     178.0       2.4
     212.0     100.0
     213.0      15.7
     214.0      33.8
     215.0       5.4

Assign. Shift(ppm) A 8.785 B 8.367 C *1 8.033 D *1 7.953 E 7.864 F 7.529 G *2 7.49 J *2 7.47 K 7.306 ASSIGNED BY H-H AND C-H COSY.

     Hz     ppm     Int.

   3510.99   8.786    950
   3503.78   8.768     31
   3502.69   8.765     30
   3502.08   8.763     32
   3344.12   8.368   1000
   3215.09   8.045    313
   3211.79   8.037    305
   3209.96   8.032    261
   3205.44   8.021    342
   3184.20   7.968    329
   3179.08   7.955    276
   3177.73   7.952    321
   3174.56   7.944    332
   3147.46   7.876    514
   3138.92   7.855    552
   3023.56   7.566     30
   3022.71   7.564     30
   3013.43   7.541    576
   3006.35   7.523    687
   2997.44   7.501    213
   2993.53   7.491    911
   2990.97   7.484    587
   2989.62   7.481    591
   2987.55   7.476    600
   2986.21   7.473    538
   2983.76   7.466    829
   2981.08   7.460    164
   2979.74   7.456    150
   2975.34   7.445     46
   2974.00   7.442     38
   2972.29   7.438     32
   2927.73   7.326    473
   2920.41   7.308    656
   2918.70   7.304    836
   2912.11   7.287    379