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MassMS-NW-7101 1,2,3,4-tetrahydro-1-naphthylamine hydrochloride C10H13N HCl (Mass of molecular ion: 147)
Source Temperature: 200 °C Sample Temperature: 120 °C Direct, 75 eV
27.0 1.8 28.0 4.8 30.0 2.2 35.0 2.4 36.0 9.6 38.0 3.6 39.0 4.8 41.0 2.0 42.0 1.9 43.0 1.0 50.0 2.3 51.0 5.5 52.0 2.1 53.0 1.4 54.0 1.2 56.0 2.6 58.5 1.4 59.5 2.6 62.0 1.5 63.0 4.1 64.0 1.7 65.0 4.9 71.5 1.4 74.0 1.3 75.0 1.6 76.0 1.6 77.0 6.6 78.0 2.6 79.0 1.5 89.0 4.0 90.0 2.9 91.0 15.7 92.0 17.3 93.0 1.7 102.0 2.1 103.0 2.8 104.0 7.1 105.0 1.4 115.0 10.4 116.0 4.4 117.0 7.0 118.0 26.7 119.0 62.2 120.0 5.9 127.0 5.4 128.0 10.6 129.0 18.2 130.0 100.0 131.0 16.0 132.0 2.1 143.0 1.6 144.0 2.6 145.0 1.3 146.0 28.7 147.0 4.9
400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C10 H13 N 0.036 g : 0.5 ml CDCl3 1,2,3,4-tetrahydro-1-naphthylamine hydrochloride 
Assign. Shift(ppm)
A 8.69 B 7.559 C 7.211 D 7.160 E 7.107 F 4.428 G *1 2.871 J *1 2.713 K 2.17 to 2.01 L 1.783
Hz ppm Int.3473.14 8.691 782 3033.57 7.591 32 3024.54 7.568 850 3017.58 7.551 917 2894.04 7.242 73 2891.60 7.236 331 2890.38 7.233 380 2884.28 7.218 955 2882.93 7.214 983 2876.95 7.199 893 2875.49 7.196 836 2871.70 7.186 131 2868.41 7.178 583 2866.94 7.174 736 2860.84 7.159 788 2859.38 7.155 906 2853.39 7.140 370 2852.05 7.137 355 2843.99 7.117 1000 2836.43 7.098 717 2835.82 7.096 707 1786.50 4.471 36 1772.09 4.435 448 1767.33 4.423 460 1763.06 4.412 254 1762.45 4.410 255 1762.08 4.410 255 1163.21 2.911 182 1157.71 2.897 349 1152.47 2.884 194 1146.12 2.868 314 1140.63 2.855 520 1135.74 2.842 266 1130.13 2.828 39 1129.76 2.827 37 1129.27 2.826 36 1128.30 2.824 32 1098.02 2.748 272 1089.60 2.727 386 1083.74 2.712 267 1081.67 2.707 235 1072.63 2.684 269 1067.38 2.671 143 1067.02 2.670 143 1062.99 2.660 45 1062.62 2.659 46 1062.26 2.658 44 1061.65 2.657 44 1061.16 2.656 43 1060.79 2.655 43 1060.18 2.653 42 1059.69 2.652 39 1059.33 2.651 38 1058.96 2.650 37 1058.59 2.649 36 1058.23 2.648 36 1057.74 2.647 34 1057.13 2.646 33 1056.64 2.644 33 1055.91 2.643 32 859.01 2.150 281 852.66 2.134 608 848.63 2.124 587 848.02 2.122 582 842.65 2.109 498 839.48 2.101 615 834.96 2.090 441 830.81 2.079 329 828.74 2.074 374 826.29 2.068 448 823.85 2.062 433 822.51 2.059 378 817.63 2.046 284 814.09 2.038 306 810.55 2.029 233 809.08 2.025 250 804.32 2.013 194 800.66 2.004 108 799.44 2.001 105 796.39 1.993 59 795.53 1.991 68 731.20 1.830 60 730.96 1.830 60 729.61 1.826 55 724.85 1.814 140 723.51 1.811 118 719.24 1.800 392 715.09 1.790 350 712.77 1.784 300 708.74 1.774 337 702.76 1.759 233 700.68 1.754 184 699.34 1.750 198 694.34 1.738 65 693.36 1.735 75
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1H NMR 89.56 MHz C10 H13 N 0.035 g : 0.5 ml CDCl3 1,2,3,4-tetrahydro-1-naphthylamine hydrochloride Assign. Shift(ppm)
A 8.71 B 7.56 C 7.36 to 6.98 D 4.44 E 2.80 F 2.31 to 1.47
Hz ppm Int.779.81 8.708 246 684.63 7.645 53 683.56 7.633 79 682.00 7.616 150 681.63 7.611 154 680.13 7.595 208 678.50 7.576 126 677.19 7.562 142 675.75 7.546 266 673.06 7.516 270 668.00 7.459 62 654.69 7.311 70 654.31 7.306 72 653.31 7.295 57 652.75 7.289 57 652.38 7.285 62 649.50 7.253 223 647.50 7.230 232 643.75 7.188 1000 640.69 7.154 690 638.56 7.130 803 635.69 7.098 191 633.94 7.079 195 631.75 7.054 64 631.25 7.049 62 629.94 7.034 85 629.13 7.025 91 399.81 4.465 144 399.38 4.460 146 398.56 4.451 143 396.38 4.426 140 396.06 4.423 144 395.56 4.417 149 395.13 4.412 150 394.50 4.405 145 393.81 4.398 140 253.56 2.832 303 253.19 2.828 305 247.44 2.763 314 187.81 2.098 530
in CDCl3
KBr disc
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