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2-氯甲基四氢呋喃

产品名称 2-氯甲基四氢呋喃

CAS号3003-84-7

分子式C5H9ClO

分子量120.58

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  • Mass

    MS-NW-1058          
    tetrahydrofurfuryl chloride
    C5H9ClO             (Mass of molecular ion:    120)
    

       Source Temperature: 240 °C
       Sample Temperature: 170 °C
       Reservoir, 75 eV
    

          15.0       1.4
          26.0       1.7
          27.0      14.9
          28.0       1.0
          29.0       5.1
          31.0       1.1
          39.0       8.2
          40.0       2.5
          41.0      26.6
          42.0      17.5
          43.0      42.1
          44.0       1.4
          49.0       3.2
          51.0       1.0
          53.0       2.3
          54.0       1.6
          55.0       7.7
          62.0       1.7
          71.0     100.0
          72.0       4.6
          75.0       1.3
          77.0       2.5
          79.0       1.2
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C5 H9 Cl O 0.02 ml : 0.5 ml CDCl3
    tetrahydrofurfuryl chloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.15 B 3.87 C *1 3.56 D *1 3.50 E 2.24 to 1.61

         Hz     ppm     Int.
    

        371.56   4.149    146
        371.25   4.146    147
        350.50   3.914    171
        348.50   3.892    269
        347.69   3.883    141
        343.88   3.840    278
        342.81   3.828    170
        342.00   3.819    160
        318.81   3.560   1000
        313.69   3.503    600
        312.56   3.490    548
        183.19   2.046    207
        182.81   2.042    213
        179.75   2.008    235
        179.25   2.002    240
        176.75   1.974    339
        174.56   1.950    197
        173.31   1.936    347
        172.81   1.930    343
        172.19   1.923    270
        171.44   1.915    214
        170.00   1.899    195
        169.19   1.890    185
        168.44   1.881    253
        167.56   1.871    194
        166.63   1.861    261
        164.88   1.842    149
        164.31   1.835    149
        159.94   1.786    155
    

in CDCl3



CCl4 solution



liquid film