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MassMS-NW-9944 1-fluorononane C9H19F (Mass of molecular ion: 146)
Source Temperature: 220 °C Sample Temperature: 160 °C Reservoir, 75 eV
27.0 13.0 28.0 3.7 29.0 26.7 33.0 1.7 39.0 10.1 40.0 1.9 41.0 52.5 42.0 22.1 43.0 100.0 44.0 4.2 47.0 8.0 53.0 2.9 54.0 2.6 55.0 61.2 56.0 43.5 57.0 53.6 58.0 2.5 59.0 3.5 61.0 14.9 67.0 3.2 68.0 3.0 69.0 28.4 70.0 35.8 71.0 30.8 72.0 1.7 73.0 1.3 74.0 2.5 75.0 7.3 82.0 5.7 83.0 23.8 84.0 30.1 85.0 17.4 86.0 1.1 88.0 2.6 89.0 2.1 96.0 2.0 97.0 26.8 98.0 11.4 102.0 1.8 103.0 1.5 111.0 1.0 117.0 1.2 126.0 1.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H19 F 0.05 ml : 0.5 ml CDCl3 1-fluorononane 
Assign. Shift(ppm)
A 4.422 B 1.680 C 1.39 D 1.34 E 1.29 F 0.884 J(A,F-19)=47.5HZ J(B,F-19)=24.8HZ J(A,B)=6.2HZ
Hz ppm Int.1797.49 4.498 303 1791.26 4.483 574 1785.03 4.467 311 1750.00 4.379 303 1743.77 4.364 573 1737.55 4.348 314 698.49 1.748 45 692.14 1.732 127 685.67 1.716 153 683.72 1.711 130 679.20 1.700 80 677.49 1.696 161 673.83 1.687 53 671.26 1.680 79 667.36 1.670 125 660.89 1.654 154 658.94 1.649 129 654.54 1.638 79 652.71 1.634 159 646.48 1.618 67 572.02 1.432 42 570.07 1.427 46 564.09 1.412 120 562.50 1.408 119 557.01 1.394 184 553.83 1.386 159 551.27 1.380 140 548.58 1.373 166 542.24 1.357 148 535.40 1.340 204 534.06 1.337 201 529.66 1.326 261 517.94 1.296 702 515.50 1.290 703 511.72 1.281 773 360.60 0.903 352 353.76 0.886 1000 346.68 0.868 430
in CDCl3
liquid film
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