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MS-IW-7442 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-1-decene C10H3F17 (Mass of molecular ion: 446)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 2.9 31.0 1.3 51.0 17.5 57.0 1.1 69.0 15.3 75.0 1.8 77.0 100.0 78.0 3.8 95.0 1.3 100.0 3.1 108.0 2.2 119.0 5.3 127.0 2.9 131.0 6.0 145.0 1.5 169.0 2.5 181.0 1.4 357.0 1.5 381.0 2.3 427.0 1.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H3 F17 0.05 ml : 0.5 ml CDCl3 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluoro-1-decene Assign. Shift(ppm)
A 5.98 B 5.97 C 5.79
Hz ppm Int.
2414.43 6.042 22 2405.27 6.019 30 2400.02 6.006 32 2397.58 6.000 136 2386.47 5.972 882 2384.52 5.967 425 2381.47 5.959 1000 2373.05 5.938 152 2369.26 5.929 123 2367.43 5.924 33 2355.83 5.895 33 2334.11 5.841 53 2321.53 5.809 553 2319.09 5.803 301 2316.41 5.797 317 2315.31 5.794 254 2313.35 5.789 194 2311.52 5.784 192 2310.06 5.781 426
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