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MS-IW-8987 3'-fluoro-4'-methoxyacetophenone C9H9FO2 (Mass of molecular ion: 168)
Source Temperature: 210 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.3 28.0 1.0 31.0 1.0 43.0 11.9 50.0 1.9 51.0 1.9 57.0 1.6 62.0 1.0 63.0 2.7 68.0 1.1 74.0 1.1 75.0 2.8 77.0 6.2 81.0 3.2 82.0 7.9 83.0 1.4 94.0 2.1 95.0 15.1 96.0 2.3 97.0 2.3 110.0 8.8 111.0 1.1 125.0 20.3 126.0 1.7 138.0 1.1 153.0 100.0 154.0 8.8 168.0 36.2 169.0 3.6
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H9 F O2 0.040 g : 0.5 ml CDCl3 3'-fluoro-4'-methoxyacetophenone Assign. Shift(ppm)
A 7.737 B 7.687 C 7.000 D 3.956 E 2.552
Hz ppm Int.
3098.14 7.753 53 3097.05 7.750 55 3096.07 7.747 62 3094.97 7.745 60 3089.60 7.731 56 3088.50 7.729 55 3087.52 7.726 69 3086.43 7.723 71 3079.10 7.705 114 3077.03 7.700 84 3067.26 7.675 112 3065.19 7.670 93 2806.03 7.022 74 2797.73 7.001 128 2789.43 6.980 72 1581.18 3.957 819 1019.90 2.552 1000 1016.72 2.545 27 0.00 0.001 219
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