1,9-二溴壬烷

Mass

MS-NW-5659          
1,9-dibromononane
C9H18Br2            (Mass of molecular ion:    284)

   Source Temperature: 280 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       1.0
      26.0       1.5
      27.0      27.6
      28.0       2.8
      29.0      23.9
      39.0      20.3
      40.0       3.5
      41.0      74.8
      42.0      12.1
      43.0      38.9
      44.0       1.3
      51.0       1.3
      53.0       6.6
      54.0       5.0
      55.0     100.0
      56.0       8.4
      57.0      61.1
      58.0       3.0
      67.0       6.5
      68.0       3.6
      69.0      84.8
      70.0       7.4
      71.0      24.1
      72.0       1.5
      81.0       3.6
      82.0       2.6
      83.0      40.8
      84.0       3.3
      85.0       4.3
      93.0       1.5
      95.0       1.6
      97.0       4.6
     107.0       5.3
     109.0       5.1
     121.0       2.2
     123.0       2.0
     125.0      11.5
     126.0       1.3
     135.0      26.9
     136.0       2.0
     137.0      25.0
     138.0       1.2
     148.0       1.5
     149.0      10.2
     150.0       2.0
     151.0       8.8
     162.0       1.0
     163.0       6.6
     164.0       1.3
     165.0       6.4
     205.0       2.4
     207.0       2.4

Assign. Shift(ppm) A 3.399 B 1.86 C 1.5 D 1.43 to 1.23 J(A,B)=6.7HZ.

     Hz     ppm     Int.

    311.69   3.481    394
    305.00   3.406   1000
    298.31   3.331    563
    173.00   1.932     95
    166.38   1.858    156
    165.94   1.853    155
    162.56   1.816     80
    159.38   1.780    141
    155.88   1.741     49
    155.75   1.740     49
    153.63   1.716     51
    153.06   1.710     51
    141.69   1.583     30
    141.31   1.578     32
    141.00   1.575     32
    140.75   1.572     32
    140.31   1.567     33
    139.38   1.557     35
    138.81   1.550     35
    136.44   1.524    102
    134.31   1.500    103
    133.88   1.495    100
    130.19   1.454    105
    128.00   1.430    106
    118.56   1.324    943
    110.63   1.236     42