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1,8-二溴辛烷

产品名称 1,8-二溴辛烷

CAS号4549-32-0

分子式C8H16Br2

分子量272.02

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  • Mass

    MS-NW-2109          
    1,8-dibromooctane
    C8H16Br2            (Mass of molecular ion:    270)
    

       Source Temperature: 260 °C
       Sample Temperature: 170 °C
       Reservoir, 75 eV
    

          18.0       1.4
          26.0       1.3
          27.0      20.4
          28.0       2.3
          29.0      15.9
          39.0      13.7
          40.0       2.3
          41.0      58.1
          42.0       8.7
          43.0      33.1
          44.0       1.2
          53.0       4.6
          54.0       4.5
          55.0      81.5
          56.0       9.9
          57.0      48.3
          58.0       2.1
          67.0       6.6
          68.0       5.1
          69.0     100.0
          70.0       5.9
          71.0      11.2
          81.0       3.9
          82.0       2.8
          83.0       8.4
          93.0       1.2
          95.0       1.1
         107.0       5.5
         109.0       5.4
         111.0      53.4
         112.0       4.8
         121.0       2.1
         123.0       1.8
         135.0      29.3
         136.0       1.7
         137.0      27.8
         138.0       1.2
         148.0       3.8
         149.0       8.2
         150.0       4.1
         151.0       7.9
         191.0       7.2
         192.0       1.1
         193.0       7.3
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C8 H16 Br2 0.04 ml : 0.5 ml CDCl3
    1,8-dibromooctane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.401 B 1.86 C 1.49 D 1.34

         Hz     ppm     Int.
    

        311.88   3.483    404
        308.19   3.442     37
        305.19   3.408   1000
        298.50   3.333    567
        179.69   2.007     34
        178.69   1.996     37
        178.00   1.988     39
        177.25   1.980     40
        176.19   1.968     51
        174.31   1.947     90
        173.06   1.933    105
        171.44   1.915     94
        169.75   1.896     91
        166.75   1.862    167
        159.94   1.786    143
        156.06   1.743     56
        155.25   1.734     47
        154.88   1.730     48
        154.56   1.726     50
        153.81   1.718     49
        153.31   1.712     51
        142.25   1.589     34
        141.56   1.581     36
        141.00   1.575     37
        140.00   1.564     41
        137.81   1.539     86
        135.38   1.512     90
        134.00   1.497     90
        133.56   1.492     90
        132.19   1.476    101
        130.94   1.463    116
        128.88   1.440    127
        128.56   1.436    126
        120.88   1.350    497
        119.88   1.339    580
        113.25   1.265     47
    

in CDCl3



liquid film



4880 A,200 M,liquid