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MS-NW-6916 o-fluorobenzamide C7H6FNO (Mass of molecular ion: 139)
Source Temperature: 280 °C Sample Temperature: 190 °C Reservoir, 75 eV
31.0 1.3 37.0 2.2 38.0 2.1 39.0 2.3 44.0 8.7 49.0 1.6 50.0 9.2 51.0 4.9 52.0 1.1 55.5 1.8 57.0 2.4 61.0 1.8 62.0 1.9 63.0 2.5 68.0 4.4 69.0 6.0 70.0 3.7 73.0 1.5 74.0 6.9 75.0 23.2 76.0 3.3 83.0 2.0 92.0 1.3 93.0 1.8 94.0 5.2 95.0 45.4 96.0 8.9 121.0 3.5 122.0 1.2 123.0 100.0 124.0 8.3 139.0 62.1 140.0 5.6
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C7 H6 F N O 0.040 g : 0.5 ml DMSO-d6 o-fluorobenzamide Assign. Shift(ppm)
A *1 7.75 B 7.685 C *1 7.68 D 7.530 E 7.28
Hz ppm Int.
3095.21 7.745 177 3080.32 7.708 269 3078.61 7.704 304 3073.00 7.690 521 3071.04 7.685 630 3065.80 7.672 285 3065.06 7.670 301 3063.48 7.666 330 3021.24 7.560 134 3019.41 7.556 137 3015.99 7.547 147 3014.04 7.542 284 3012.82 7.539 206 3012.08 7.537 203 3011.11 7.535 184 3008.54 7.528 205 3007.81 7.527 208 3006.35 7.523 281 3005.74 7.521 245 3003.78 7.517 176 3000.37 7.508 181 2998.54 7.503 162 2919.31 7.305 368 2917.36 7.300 420 2916.26 7.298 355 2909.91 7.282 705 2908.81 7.279 1000 2904.79 7.269 46 2902.34 7.263 295 2901.25 7.260 539
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