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网站主页CAS数据库列表 4432-77-3更多图谱N-叔丁基乙胺(4432-77-3)核磁图(1HNMR)

N-叔丁基乙胺

产品名称 N-叔丁基乙胺

CAS号4432-77-3

分子式C6H15N

分子量101.19

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  • Mass

    MS-NW-3359          
    N-ethyl-tert-butylamine
    C6H15N              (Mass of molecular ion:    101)
    

       Source Temperature: 280 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          15.0       2.4
          18.0       2.4
          27.0       4.5
          28.0       3.3
          29.0       7.8
          30.0      16.9
          39.0       3.9
          41.0      10.7
          42.0       9.1
          43.0       1.4
          44.0       9.5
          55.0       1.9
          56.0       2.2
          57.0       9.8
          58.0      37.1
          59.0       2.3
          70.0       2.1
          71.0       1.0
          84.0       1.2
          86.0     100.0
          87.0       6.2
         101.0       3.1
    

400 MHz in CDCl3

90 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C6 H15 N 0.05 ml : 0.5 ml CDCl3
    N-ethyl-tert-butylamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.603 B 1.104 C 1.099 D 1.

         Hz     ppm     Int.
    

       1051.27   2.631    100
       1044.07   2.613    271
       1036.99   2.595    278
       1029.91   2.578    109
        446.66   1.118    358
        441.16   1.104   1000
        439.21   1.099    700
        432.13   1.082    334
        378.30   0.947     21
    


  • 1H NMR 89.56 MHz
    C6 H15 N 0.04 ml : 0.5 ml CDCl3
    N-ethyl-tert-butylamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.60 B 1.101 C 1.101 D 0.76

         Hz     ppm     Int.
    

        236.63   2.643     53
        229.56   2.564     59
        105.06   1.174     68
        100.56   1.123     28
         98.63   1.102   1000
         90.88   1.015     50
    

in CDCl3



liquid film