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MassMS-NW-1211 1-methyl-1,4-diazacycloheptane C6H14N2 (Mass of molecular ion: 114)
Source Temperature: 250 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 8.1 18.0 4.3 26.0 1.1 27.0 6.0 28.0 15.7 29.0 3.9 30.0 9.0 39.0 4.0 40.0 1.5 41.0 11.8 42.0 41.6 43.0 40.1 44.0 40.7 45.0 1.8 46.0 1.6 54.0 2.3 55.0 2.1 56.0 10.3 57.0 35.9 58.0 100.0 59.0 4.1 68.0 2.6 69.0 7.7 70.0 26.7 71.0 12.7 72.0 31.9 73.0 1.7 82.0 2.3 83.0 11.9 84.0 19.0 85.0 10.5 86.0 1.7 99.0 2.6 113.0 3.3 114.0 38.7 115.0 3.0
90 MHz in CDCl3
400 MHz in CDCl3
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1H NMR 89.56 MHz C6 H14 N2 0.05 ml : 0.5 ml CDCl3 1-methyl-1,4-diazacycloheptane 
Assign. Shift(ppm)
A 2.93 B 2.60 C 2.380 D 1.77 E 1.74 400MHZ : HSP-40-459
Hz ppm Int.270.69 3.023 128 266.31 2.974 117 264.63 2.955 249 262.75 2.934 141 261.75 2.923 124 258.44 2.886 240 256.94 2.869 127 255.06 2.848 95 240.63 2.687 106 237.25 2.650 120 235.31 2.628 211 233.81 2.611 155 229.31 2.561 215 226.06 2.525 85 213.19 2.381 1000 171.38 1.914 37 167.25 1.868 42 165.38 1.847 93 163.75 1.829 43 161.50 1.804 56 159.44 1.781 113 155.44 1.736 250
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1H NMR 399.65 MHz C6 H14 N2 0.05 ml : 0.5 ml CDCl3 1-methyl-1,4-diazacycloheptane Assign. Shift(ppm)
A 2.955 B 2.921 C 2.621 D 2.585 E 2.385 F 1.793 G 1.69 ASSIGNED BY H-H COSY. 90MHZ : HSP-00-595
Hz ppm Int.1187.50 2.972 227 1181.40 2.957 299 1179.32 2.951 46 1178.22 2.949 32 1175.05 2.941 237 1172.36 2.934 205 1169.68 2.927 68 1168.82 2.925 96 1167.36 2.921 166 1165.41 2.917 88 1164.43 2.914 67 1162.11 2.908 215 1053.59 2.637 146 1050.78 2.630 43 1047.73 2.622 155 1044.31 2.614 46 1041.75 2.607 158 1038.09 2.598 160 1034.91 2.590 82 1032.71 2.585 150 1030.88 2.580 80 1027.59 2.572 123 955.32 2.391 71 953.13 2.385 1000 950.20 2.378 48 728.39 1.823 66 723.88 1.812 45 722.29 1.808 108 719.97 1.802 39 717.90 1.797 58 716.55 1.793 135 716.06 1.792 135 714.97 1.789 60 712.89 1.784 36 710.33 1.778 97 708.86 1.774 40 704.35 1.763 56 676.15 1.692 37
in CDCl3
CCl4 solution
liquid film
4880 A,200 M,liquid
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