4-氨基-9-芴酮

Mass

MS-NW-6466          
4-amino-9-fluorenone
C13H9NO             (Mass of molecular ion:    195)

   Source Temperature: 180 °C
   Sample Temperature: 100 °C
   Direct, 75 eV

      18.0       2.6
      28.0       1.1
      39.0       1.3
      51.0       1.0
      62.0       1.0
      63.0       2.2
      69.5       3.2
      70.0       1.7
      70.5       3.0
      74.0       1.1
      75.0       1.0
      82.5       1.7
      83.5       6.4
      84.0       1.3
      87.0       1.3
      89.0       1.4
      97.5       2.6
     113.0       1.6
     114.0       1.4
     115.0       1.5
     138.0       1.1
     139.0      11.7
     140.0       6.3
     141.0       1.0
     164.0       1.3
     166.0      14.8
     167.0      26.6
     168.0       4.2
     194.0       2.1
     195.0     100.0
     196.0      14.8
     197.0       1.2

Assign. Shift(ppm) A 7.876 B 7.59 C 7.56 D 7.271 E 7.118 F *1 6.97 G *1 6.95 J 5.76

     Hz     ppm     Int.

   3151.61   7.886    558
   3144.17   7.868    635
   3036.74   7.599    515
   3030.15   7.583    801
   3029.42   7.581    781
   3025.51   7.571     58
   3022.83   7.564    622
   3021.61   7.561    506
   3015.26   7.545    322
   3014.04   7.542    266
   2913.21   7.290    383
   2912.72   7.289    385
   2905.64   7.271    656
   2901.98   7.262     36
   2898.44   7.253    309
   2897.83   7.251    296
   2853.27   7.140    373
   2846.19   7.122    527
   2845.21   7.120    539
   2838.13   7.102    596
   2790.89   6.984    642
   2790.04   6.982    696
   2782.71   6.963    587
   2781.74   6.961    638
   2780.64   6.958    808
   2776.37   6.948     56
   2773.68   6.941    625
   2773.07   6.939    514
   2301.15   5.758   1000