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MassMS-NW-0472 9-fluorenone C13H8O (Mass of molecular ion: 180)
Source Temperature: 170 °C Sample Temperature: 120 °C Direct, 75 eV
39.0 1.4 50.0 2.4 51.0 2.0 62.0 1.8 63.0 6.2 74.0 3.5 75.0 5.0 75.5 1.6 76.0 13.4 76.5 1.5 77.0 1.2 86.0 1.3 87.0 1.8 90.0 2.1 98.0 1.8 99.0 1.6 102.0 1.4 125.0 1.5 126.0 5.1 150.0 7.2 151.0 13.0 152.0 28.9 153.0 3.8 180.0 100.0 181.0 15.4 182.0 1.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C13 H8 O 0.032 g : 0.5 ml CDCl3 9-fluorenone 
Assign. Shift(ppm)
A 7.638 B 7.48 C 7.47 D 7.274
Hz ppm Int.3060.55 7.659 34 3059.33 7.656 38 3057.01 7.650 372 3056.15 7.648 553 3055.18 7.645 376 3053.22 7.640 40 3052.12 7.637 43 3049.68 7.631 409 3048.83 7.629 533 3047.73 7.626 394 3001.71 7.511 31 3000.37 7.508 35 2998.17 7.502 140 2997.31 7.500 155 2996.58 7.499 225 2995.85 7.497 219 2990.72 7.484 661 2989.99 7.482 669 2989.14 7.480 665 2988.28 7.478 1000 2987.18 7.475 565 2983.76 7.466 56 2981.32 7.460 569 2980.22 7.458 538 2977.54 7.451 37 2976.32 7.448 38 2973.88 7.442 221 2972.78 7.439 204 2916.50 7.298 31 2914.18 7.292 381 2912.48 7.288 366 2909.67 7.281 42 2907.23 7.275 402 2906.86 7.274 414 2905.52 7.271 405 2899.90 7.257 273 2898.32 7.253 270
in CDCl3
CCl4 solution
KBr disc
nujol mull
ANION RADICAL, REDUCTION WITH NA METAL IN DME
ANION RADICAL, REDUCTION WITH NA IN THF, ENDOR
ANION RADICAL, ELECTROREDUCTION IN DMF
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