-
MassMS-IW-3593 (S)-(+)-1,2-propanediol C3H8O2 (Mass of molecular ion: 76)
Source Temperature: 220 °C Sample Temperature: 160 °C Reservoir, 75 eV
15.0 6.0 19.0 8.5 26.0 2.2 27.0 17.7 28.0 6.1 29.0 14.7 30.0 1.4 31.0 22.4 32.0 1.0 33.0 3.1 39.0 2.6 41.0 4.1 42.0 3.9 43.0 33.2 44.0 13.1 45.0 100.0 46.0 5.6 57.0 5.2 58.0 1.9 59.0 1.9 61.0 13.1 76.0 1.9
400 MHz in CDCl3
-
1H NMR 399.65 MHz C3 H8 O2 0.05 ml : 0.5 ml CDCl3 (S)-(+)-1,2-propanediol 
Assign. Shift(ppm)
A 4.56 B 3.855 C *1 3.552 D *1 3.371 E 1.126 J(B,C)=3.1HZ J(B,D)=7.7HZ
Hz ppm Int.1822.27 4.560 498 1549.44 3.877 71 1548.34 3.875 52 1546.39 3.870 80 1542.97 3.861 86 1541.87 3.859 99 1539.92 3.854 95 1538.70 3.851 91 1535.40 3.842 84 1532.35 3.835 76 1427.61 3.573 114 1424.56 3.565 109 1416.26 3.544 150 1413.21 3.537 138 1355.96 3.393 200 1348.27 3.374 190 1344.60 3.365 157 1336.91 3.346 142 453.37 1.135 1000 446.90 1.119 907
in CDCl3
liquid film
更多供应商
