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MassMS-IW-1292 (iodomethyl)trimethylsilane C4H11ISi (Mass of molecular ion: 214)
Source Temperature: 240 °C Sample Temperature: 160 °C Reservoir, 75 eV
28.0 1.6 29.0 2.8 31.0 1.0 42.0 2.4 43.0 9.3 44.0 3.0 45.0 4.7 53.0 1.2 55.0 1.5 57.0 1.1 58.0 1.2 59.0 3.1 72.0 3.9 73.0 26.5 74.0 2.3 155.0 5.2 157.0 2.7 169.0 1.4 170.0 3.7 171.0 74.4 172.0 4.8 173.0 2.6 185.0 2.4 199.0 100.0 200.0 8.5 201.0 3.6 214.0 44.9 215.0 4.3 216.0 1.6
400 MHz in CDCl3
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1H NMR 399.65 MHz C4 H11 I Si 0.05 ml : 0.5 ml CDCl3 (iodomethyl)trimethylsilane 
Assign. Shift(ppm)
A 2.002 B 0.152
Hz ppm Int.800.17 2.003 553 120.61 0.302 21 71.41 0.179 29 64.82 0.163 235 61.04 0.153 1000 57.98 0.146 350 51.76 0.130 53 0.98 0.003 25
in CDCl3
liquid film
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