2-甲基-4-甲氧基二苯胺

产品名称 2-甲基-4-甲氧基二苯胺

CAS号41317-15-1

分子式C14H15NO

分子量213.27

¹³CNMR

Mass

MS-KW-0183          
4-methoxy-2-methyldiphenylamine
C14H15NO            (Mass of molecular ion:    213)

   Source Temperature: 140 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      39.0       1.8
      51.0       3.8
      52.0       1.4
      63.0       1.0
      65.0       2.2
      76.0       1.1
      77.0       6.9
      78.0       1.7
      83.5       3.1
      90.0       2.1
      90.5       2.0
      91.0       1.2
      92.0       1.1
      99.0       2.5
     103.0       1.0
     105.5       1.4
     106.0       1.2
     106.5       7.0
     107.0       1.2
     115.0       1.1
     128.0       2.7
     130.0       2.1
     143.0       1.2
     154.0       3.4
     155.0       2.7
     167.0       3.6
     168.0       3.6
     169.0       1.6
     170.0       2.1
     180.0       4.8
     181.0       2.6
     182.0       1.2
     183.0       1.1
     196.0       1.9
     197.0       1.4
     198.0     100.0
     199.0      14.8
     200.0       1.3
     210.0       1.5
     212.0       2.2
     213.0      92.9
     214.0      14.8
     215.0       1.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₄ H₁₅ N O	0.038 g : 0.5 ml CDCl₃
4-methoxy-2-methyldiphenylamine

    Assign.     Shift(ppm)

      A             7.166
      B             7.125
      C             6.79
      D             6.77
      E             6.72
      F             6.70
      G             5.16
      J             3.778
      K             2.202

     Hz     ppm     Int.

   2872.31   7.188    124
   2871.46   7.185     50
   2870.24   7.182     44
   2864.99   7.169    162
   2863.77   7.166    157
   2858.40   7.153     52
   2857.18   7.150     59
   2856.32   7.148    147
   2852.05   7.137    123
   2843.38   7.115    132
   2715.58   6.795     85
   2712.89   6.789    125
   2711.91   6.786    130
   2710.82   6.783     53
   2705.57   6.770     52
   2704.47   6.768    115
   2703.49   6.765     58
   2698.24   6.752     32
   2697.14   6.749     58
   2696.04   6.747     35
   2690.06   6.732     64
   2689.58   6.730     65
   2687.01   6.724     53
   2686.65   6.723     53
   2681.40   6.710     89
   2680.30   6.707    179
   2679.08   6.704    205
   2678.34   6.702    137
   2677.12   6.699     63
   2673.58   6.690     55
   2672.61   6.688     89
   2671.63   6.685    169
   2670.53   6.683    145
   2064.33   5.166     34
   1509.89   3.779   1000
    880.00   2.202    535

in CDCl3

KBr disk

Nujol

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