2-甲氧基-5-甲基苯胺

产品名称 2-甲氧基-5-甲基苯胺

CAS号120-71-8

分子式C8H11NO

分子量137.18

¹³CNMR

Mass

MS-NW-4784          
5-methyl-o-anisidine
C8H11NO             (Mass of molecular ion:    137)

   Source Temperature: 260 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      15.0       1.7
      27.0       2.0
      28.0       3.5
      38.0       1.4
      39.0       6.0
      40.0       1.5
      41.0       4.3
      42.0       3.1
      50.0       1.4
      51.0       4.0
      52.0       3.3
      53.0       2.8
      54.0       2.9
      63.0       1.4
      65.0       4.6
      66.0       5.8
      67.0       5.9
      77.0      16.5
      78.0       3.5
      79.0       3.8
      91.0       1.2
      92.0       1.7
      93.0       8.5
      94.0      48.6
      95.0       3.9
     104.0       1.5
     106.0       4.0
     108.0       1.1
     121.0       2.9
     122.0     100.0
     123.0       8.4
     136.0       1.4
     137.0      72.8
     138.0       6.7

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₈ H₁₁ N O	0.043 g : 0.5 ml CDCl₃
5-methyl-o-anisidine

    Assign.     Shift(ppm)

      A             2.205
      B             3.65
      C             3.791
      D          6.41 to 6.57
      E             6.65

     Hz     ppm     Int.

    601.81   6.720     46
    595.50   6.650     27
    593.06   6.622    154
    587.25   6.558     24
    586.56   6.550     30
    585.19   6.535    171
    584.63   6.528    223
    584.00   6.521    153
    582.88   6.509     73
    582.25   6.502     64
    578.44   6.459     33
    577.81   6.452     33
    339.56   3.792   1000
    327.25   3.654    503
    197.56   2.206    594

in CDCl3

CCl4 solution

KBr disc

nujol mull

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