-
MassMS-IW-1100 2,3,6,7-tetrahydro-1H,5H-pyrido(3,2,1-ij)quinolin-8-ol C12H15NO (Mass of molecular ion: 189)
Source Temperature: 160 °C Sample Temperature: 140 °C Direct, 75 eV
39.0 1.2 51.0 1.3 65.0 1.1 77.0 2.4 79.5 1.2 80.5 2.8 91.0 1.2 93.5 1.8 94.5 2.4 115.0 1.1 117.0 1.9 130.0 1.9 131.0 1.0 132.0 1.9 133.0 1.6 144.0 1.1 146.0 3.8 147.0 1.0 158.0 2.1 159.0 1.1 160.0 15.7 161.0 3.3 170.0 1.1 172.0 3.4 173.0 1.8 174.0 5.7 186.0 4.1 187.0 1.7 188.0 71.9 189.0 100.0 190.0 13.2 191.0 1.0 229.0 1.0
400 MHz in CDCl3
-
1H NMR 399.65 MHz C12 H15 N O 0.044 g : 0.5 ml CDCl3 2,3,6,7-tetrahydro-1H,5H-pyrido(3,2,1-ij)quinolin-8-ol 
Assign. Shift(ppm)
A 6.629 B 6.026 C 4.6 D 3.068 E 2.66 F 1.958
Hz ppm Int.2654.42 6.642 231 2653.69 6.641 347 2652.95 6.639 263 2649.17 6.629 32 2646.36 6.622 249 2645.63 6.620 375 2644.90 6.619 282 2412.35 6.037 669 2404.30 6.017 627 1244.14 3.114 49 1234.74 3.090 547 1232.18 3.084 223 1229.00 3.076 959 1226.56 3.070 324 1223.51 3.062 1000 1219.97 3.053 189 1217.77 3.048 565 1076.42 2.694 362 1069.95 2.678 644 1062.50 2.659 559 1055.18 2.641 740 1048.46 2.624 411 799.07 2.000 211 796.88 1.994 110 794.80 1.989 163 793.33 1.986 269 792.36 1.983 454 790.28 1.978 201 787.84 1.972 471 786.87 1.969 456 785.52 1.966 424 783.45 1.961 292 781.13 1.955 709 778.81 1.949 280 776.49 1.943 410 774.41 1.938 513 772.22 1.933 176 769.78 1.927 355 767.70 1.921 144 765.63 1.916 71 763.18 1.910 166
KBr disc
nujol mull
更多供应商
