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网站主页CAS数据库列表 41175-50-2更多图谱8-羟基久洛里定(41175-50-2)Raman光谱

8-羟基久洛里定

产品名称 8-羟基久洛里定

CAS号41175-50-2

分子式C12H15NO

分子量189.25

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  • Mass

    MS-IW-1100          
    2,3,6,7-tetrahydro-1H,5H-pyrido(3,2,1-ij)quinolin-8-ol
    C12H15NO            (Mass of molecular ion:    189)
    

       Source Temperature: 160 °C
       Sample Temperature: 140 °C
       Direct, 75 eV
    

          39.0       1.2
          51.0       1.3
          65.0       1.1
          77.0       2.4
          79.5       1.2
          80.5       2.8
          91.0       1.2
          93.5       1.8
          94.5       2.4
         115.0       1.1
         117.0       1.9
         130.0       1.9
         131.0       1.0
         132.0       1.9
         133.0       1.6
         144.0       1.1
         146.0       3.8
         147.0       1.0
         158.0       2.1
         159.0       1.1
         160.0      15.7
         161.0       3.3
         170.0       1.1
         172.0       3.4
         173.0       1.8
         174.0       5.7
         186.0       4.1
         187.0       1.7
         188.0      71.9
         189.0     100.0
         190.0      13.2
         191.0       1.0
         229.0       1.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C12 H15 N O 0.044 g : 0.5 ml CDCl3
    2,3,6,7-tetrahydro-1H,5H-pyrido(3,2,1-ij)quinolin-8-ol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.629 B 6.026 C 4.6 D 3.068 E 2.66 F 1.958

         Hz     ppm     Int.
    

       2654.42   6.642    231
       2653.69   6.641    347
       2652.95   6.639    263
       2649.17   6.629     32
       2646.36   6.622    249
       2645.63   6.620    375
       2644.90   6.619    282
       2412.35   6.037    669
       2404.30   6.017    627
       1244.14   3.114     49
       1234.74   3.090    547
       1232.18   3.084    223
       1229.00   3.076    959
       1226.56   3.070    324
       1223.51   3.062   1000
       1219.97   3.053    189
       1217.77   3.048    565
       1076.42   2.694    362
       1069.95   2.678    644
       1062.50   2.659    559
       1055.18   2.641    740
       1048.46   2.624    411
        799.07   2.000    211
        796.88   1.994    110
        794.80   1.989    163
        793.33   1.986    269
        792.36   1.983    454
        790.28   1.978    201
        787.84   1.972    471
        786.87   1.969    456
        785.52   1.966    424
        783.45   1.961    292
        781.13   1.955    709
        778.81   1.949    280
        776.49   1.943    410
        774.41   1.938    513
        772.22   1.933    176
        769.78   1.927    355
        767.70   1.921    144
        765.63   1.916     71
        763.18   1.910    166
    



KBr disc



nujol mull