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网站主页CAS数据库列表 40807-61-2更多图谱4-苯基-4-羟基哌啶(40807-61-2)红外图谱(IR1)

4-苯基-4-羟基哌啶

产品名称 4-苯基-4-羟基哌啶

CAS号40807-61-2

分子式C11H15NO

分子量177.24

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  • Mass

    MS-IW-9831          
    4-phenyl-4-piperidinol
    C11H15NO            (Mass of molecular ion:    177)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       2.7
          17.0       3.0
          18.0      14.2
          27.0       6.0
          28.0      12.6
          29.0       6.0
          30.0      15.2
          39.0       6.5
          41.0       5.7
          42.0     100.0
          43.0      11.3
          44.0      10.1
          50.0       4.7
          51.0      13.7
          52.0       3.6
          53.0       4.3
          54.0       1.7
          55.0       3.2
          56.0      20.7
          57.0      21.4
          58.0       2.0
          60.0       1.1
          62.0       1.4
          63.0       5.2
          64.0       3.0
          64.5       1.0
          65.0       5.3
          68.0       5.3
          74.0       2.3
          75.0       2.6
          76.0       3.3
          77.0      18.4
          77.5       2.6
          78.0       6.6
          78.5       1.9
          79.0       2.1
          79.5       1.2
          80.0       6.1
          81.0       2.5
          82.0      28.3
          83.0       1.8
          89.0       2.6
          91.0      20.7
          92.0       2.3
         101.0       1.2
         102.0       6.2
         103.0       7.7
         104.0       5.3
         105.0       5.8
         106.0       1.6
         115.0      25.1
         116.0       6.4
         117.0       8.2
         118.0       2.0
         120.0       2.0
         126.0       1.3
         127.0       6.6
         128.0      12.5
         129.0      22.3
         130.0      33.7
         131.0      10.6
         132.0       2.3
         133.0       1.4
         141.0       2.1
         143.0       2.8
         144.0       3.3
         154.0       6.0
         155.0      16.3
         156.0       5.6
         157.0       1.8
         158.0      43.0
         159.0      77.1
         160.0      10.0
         176.0       1.1
         177.0       3.4
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C11 H15 N O 0.039 g : 0.5 ml DMSO-d6
    4-phenyl-4-piperidinol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.472 B 7.309 C 7.191 D 4.9 E 2.931 F 2.710 G 1.787 J 1.504

         Hz     ppm     Int.
    

       2999.02   7.505     30
       2998.54   7.503     30
       2991.58   7.486    634
       2990.36   7.483    803
       2983.15   7.465    914
       2982.30   7.463    872
       2928.83   7.329    562
       2927.12   7.325    255
       2921.39   7.310   1000
       2913.45   7.291    598
       2880.98   7.209    223
       2879.76   7.206    362
       2878.66   7.203    241
       2872.56   7.188    514
       2866.33   7.173    133
       2865.23   7.170    200
       2864.14   7.167    125
       1184.33   2.964    239
       1182.01   2.958    265
       1172.36   2.934    540
       1169.92   2.928    534
       1160.16   2.903    345
       1157.96   2.898    308
       1089.97   2.728    403
       1079.35   2.701    310
        729.25   1.825    209
        724.73   1.814    226
        716.55   1.793    411
        712.28   1.783    394
        704.10   1.762    257
        699.58   1.751    226
        606.45   1.518    520
        594.48   1.488    420
    

in DMSO-d6



KBr disc



nujol mull