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MassMS-IW-9831 4-phenyl-4-piperidinol C11H15NO (Mass of molecular ion: 177)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 2.7 17.0 3.0 18.0 14.2 27.0 6.0 28.0 12.6 29.0 6.0 30.0 15.2 39.0 6.5 41.0 5.7 42.0 100.0 43.0 11.3 44.0 10.1 50.0 4.7 51.0 13.7 52.0 3.6 53.0 4.3 54.0 1.7 55.0 3.2 56.0 20.7 57.0 21.4 58.0 2.0 60.0 1.1 62.0 1.4 63.0 5.2 64.0 3.0 64.5 1.0 65.0 5.3 68.0 5.3 74.0 2.3 75.0 2.6 76.0 3.3 77.0 18.4 77.5 2.6 78.0 6.6 78.5 1.9 79.0 2.1 79.5 1.2 80.0 6.1 81.0 2.5 82.0 28.3 83.0 1.8 89.0 2.6 91.0 20.7 92.0 2.3 101.0 1.2 102.0 6.2 103.0 7.7 104.0 5.3 105.0 5.8 106.0 1.6 115.0 25.1 116.0 6.4 117.0 8.2 118.0 2.0 120.0 2.0 126.0 1.3 127.0 6.6 128.0 12.5 129.0 22.3 130.0 33.7 131.0 10.6 132.0 2.3 133.0 1.4 141.0 2.1 143.0 2.8 144.0 3.3 154.0 6.0 155.0 16.3 156.0 5.6 157.0 1.8 158.0 43.0 159.0 77.1 160.0 10.0 176.0 1.1 177.0 3.4
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C11 H15 N O 0.039 g : 0.5 ml DMSO-d6 4-phenyl-4-piperidinol 
Assign. Shift(ppm)
A 7.472 B 7.309 C 7.191 D 4.9 E 2.931 F 2.710 G 1.787 J 1.504
Hz ppm Int.2999.02 7.505 30 2998.54 7.503 30 2991.58 7.486 634 2990.36 7.483 803 2983.15 7.465 914 2982.30 7.463 872 2928.83 7.329 562 2927.12 7.325 255 2921.39 7.310 1000 2913.45 7.291 598 2880.98 7.209 223 2879.76 7.206 362 2878.66 7.203 241 2872.56 7.188 514 2866.33 7.173 133 2865.23 7.170 200 2864.14 7.167 125 1184.33 2.964 239 1182.01 2.958 265 1172.36 2.934 540 1169.92 2.928 534 1160.16 2.903 345 1157.96 2.898 308 1089.97 2.728 403 1079.35 2.701 310 729.25 1.825 209 724.73 1.814 226 716.55 1.793 411 712.28 1.783 394 704.10 1.762 257 699.58 1.751 226 606.45 1.518 520 594.48 1.488 420
in DMSO-d6
KBr disc
nujol mull
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