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MassMS-NW-8941 5-methyl-2-nitroanisole C8H9NO3 (Mass of molecular ion: 167)
Source Temperature: 250 °C Sample Temperature: 130 °C Reservoir, 75 eV
18.0 1.0 27.0 3.2 28.0 3.3 30.0 2.7 31.0 1.6 38.0 2.3 39.0 15.6 40.0 2.7 41.0 4.7 42.0 1.0 43.0 2.4 50.0 7.1 51.0 16.6 52.0 13.6 53.0 6.5 55.0 1.6 62.0 3.1 63.0 10.2 64.0 3.7 65.0 44.2 66.0 11.3 67.0 1.6 74.0 1.5 75.0 1.6 76.0 2.8 77.0 28.6 78.0 28.2 79.0 10.2 80.0 1.3 81.0 3.4 89.0 9.4 90.0 4.9 91.0 64.3 92.0 23.3 93.0 6.8 94.0 6.7 105.0 20.0 106.0 18.8 107.0 11.8 108.0 1.5 109.0 9.5 110.0 1.1 119.0 1.8 120.0 100.0 121.0 8.3 122.0 2.4 137.0 32.0 138.0 6.2 150.0 1.1 167.0 82.8 168.0 8.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H9 N O3 0.040 g : 0.5 ml CDCl3 5-methyl-2-nitroanisole 
Assign. Shift(ppm)
A 7.780 B 6.87 C 6.82 D 3.944 E 2.419
Hz ppm Int.701.31 7.831 97 693.25 7.741 118 615.19 6.870 172 612.81 6.843 47 607.00 6.778 62 606.38 6.771 65 605.38 6.760 53 604.75 6.753 44 353.25 3.945 1000 216.75 2.421 590
in CDCl3
KBr disc
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