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3-甲基-4-硝基苯甲醚

产品名称 3-甲基-4-硝基苯甲醚

CAS号5367-32-8

分子式C8H9NO3

分子量167.16

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  • Mass

    MS-NW-6903          
    3-methyl-4-nitroanisole
    C8H9NO3             (Mass of molecular ion:    167)
    

       Source Temperature: 120 °C
       Sample Temperature:  70 °C
       Direct, 75 eV
    

          15.0       4.6
          18.0       2.3
          26.0       1.6
          27.0       4.7
          28.0       3.7
          29.0       1.9
          30.0       3.7
          37.0       1.7
          38.0       5.3
          39.0      16.8
          40.0       2.7
          41.0       6.7
          42.0       1.3
          43.0       2.0
          45.0       1.3
          50.0       9.1
          51.0      21.7
          52.0      17.4
          53.0       8.8
          54.0       1.5
          55.0       3.9
          59.0       1.9
          61.0       1.6
          62.0       5.1
          63.0      13.8
          64.0       4.6
          65.0      21.2
          66.0       6.5
          67.0       3.6
          68.0       1.4
          74.0       2.6
          75.0       2.3
          76.0       2.6
          77.0      29.9
          78.0      29.8
          79.0       7.6
          80.0       3.8
          81.0       2.0
          86.0       1.0
          89.0       8.1
          90.0       8.3
          91.0      28.1
          92.0      10.1
          93.0       2.2
          94.0       6.8
          95.0      26.6
          96.0       2.3
         105.0       4.5
         106.0      14.1
         107.0       6.4
         108.0       5.8
         109.0       5.0
         120.0       2.3
         121.0       8.4
         122.0      20.7
         123.0       2.9
         134.0       1.2
         135.0       3.3
         136.0       5.3
         137.0       8.2
         138.0       1.5
         150.0     100.0
         151.0       9.9
         152.0       1.3
         167.0      84.9
         168.0       8.4
         169.0       1.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C8 H9 N O3 0.038 g : 0.5 ml CDCl3
    3-methyl-4-nitroanisole
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.076 B 6.797 C 6.78 D 3.879 E 2.627

         Hz     ppm     Int.
    

       3232.18   8.088    133
       3223.27   8.066    138
       2723.39   6.815     56
       2720.58   6.808     80
       2714.23   6.792     40
       2711.67   6.786    105
       2709.11   6.779    140
       2706.91   6.774     66
       2706.30   6.772     72
       1550.42   3.880   1000
       1049.80   2.627    611
    

in CDCl3



KBr disc



nujol mull



4880 A,200 M,powder