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MS-IW-4072 (R)-(+)-alpha-methyldibenzylamine C15H17N (Mass of molecular ion: 211)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
28.0 1.2 39.0 1.5 42.0 1.5 51.0 2.4 65.0 7.5 77.0 8.1 78.0 2.3 79.0 6.1 89.0 1.5 90.0 1.0 91.0 100.0 92.0 10.1 98.0 1.2 103.0 3.6 104.0 4.1 105.0 17.5 106.0 8.8 120.0 2.7 134.0 5.8 196.0 79.8 197.0 12.5 210.0 1.1 211.0 1.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C15 H17 N 0.05 ml : 0.5 ml CDCl3 (R)-(+)-alpha-methyldibenzylamine Assign. Shift(ppm)
A 7.33 to 7.21 B 3.776 C *1 3.626 D *1 3.568 E 1.59 F 1.336 J(C,D)=-13.2HZ
Hz ppm Int.
2937.13 7.350 67 2935.06 7.345 117 2932.74 7.339 72 2932.37 7.338 72 2928.59 7.328 738 2928.10 7.327 750 2926.64 7.324 515 2921.75 7.311 367 2921.02 7.309 457 2919.07 7.305 154 2916.50 7.298 86 2915.28 7.295 155 2913.82 7.291 147 2913.09 7.290 162 2909.91 7.282 131 2907.96 7.277 334 2907.10 7.275 300 2902.95 7.264 421 2901.25 7.260 849 2900.51 7.258 769 2896.24 7.247 110 2894.53 7.243 153 2892.82 7.239 155 2890.75 7.234 189 2888.43 7.228 89 2886.96 7.224 107 2884.89 7.219 203 2884.28 7.218 218 2882.81 7.214 181 2881.96 7.212 136 2879.39 7.205 133 2877.81 7.201 151 2875.98 7.197 166 2872.68 7.188 83 2869.87 7.181 71 2867.55 7.176 43 1519.29 3.802 72 1512.70 3.786 222 1506.10 3.769 226 1499.51 3.753 76 1458.50 3.650 146 1445.19 3.617 351 1429.93 3.578 395 1416.75 3.545 160 635.13 1.590 50 537.23 1.345 987 530.64 1.328 1000
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