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网站主页CAS数据库列表 38235-77-7更多图谱(R)-(+)-N-苄基-1-苯乙胺(38235-77-7)核磁图(1HNMR)

(R)-(+)-N-苄基-1-苯乙胺

产品名称 (R)-(+)-N-苄基-1-苯乙胺

CAS号38235-77-7

分子式C15H17N

分子量211.3

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  • Mass

    MS-IW-4072          
    (R)-(+)-alpha-methyldibenzylamine
    C15H17N             (Mass of molecular ion:    211)
    

       Source Temperature: 220 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          28.0       1.2
          39.0       1.5
          42.0       1.5
          51.0       2.4
          65.0       7.5
          77.0       8.1
          78.0       2.3
          79.0       6.1
          89.0       1.5
          90.0       1.0
          91.0     100.0
          92.0      10.1
          98.0       1.2
         103.0       3.6
         104.0       4.1
         105.0      17.5
         106.0       8.8
         120.0       2.7
         134.0       5.8
         196.0      79.8
         197.0      12.5
         210.0       1.1
         211.0       1.5
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C15 H17 N 0.05 ml : 0.5 ml CDCl3
    (R)-(+)-alpha-methyldibenzylamine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.33 to 7.21 B 3.776 C *1 3.626 D *1 3.568 E 1.59 F 1.336 J(C,D)=-13.2HZ

         Hz     ppm     Int.
    

       2937.13   7.350     67
       2935.06   7.345    117
       2932.74   7.339     72
       2932.37   7.338     72
       2928.59   7.328    738
       2928.10   7.327    750
       2926.64   7.324    515
       2921.75   7.311    367
       2921.02   7.309    457
       2919.07   7.305    154
       2916.50   7.298     86
       2915.28   7.295    155
       2913.82   7.291    147
       2913.09   7.290    162
       2909.91   7.282    131
       2907.96   7.277    334
       2907.10   7.275    300
       2902.95   7.264    421
       2901.25   7.260    849
       2900.51   7.258    769
       2896.24   7.247    110
       2894.53   7.243    153
       2892.82   7.239    155
       2890.75   7.234    189
       2888.43   7.228     89
       2886.96   7.224    107
       2884.89   7.219    203
       2884.28   7.218    218
       2882.81   7.214    181
       2881.96   7.212    136
       2879.39   7.205    133
       2877.81   7.201    151
       2875.98   7.197    166
       2872.68   7.188     83
       2869.87   7.181     71
       2867.55   7.176     43
       1519.29   3.802     72
       1512.70   3.786    222
       1506.10   3.769    226
       1499.51   3.753     76
       1458.50   3.650    146
       1445.19   3.617    351
       1429.93   3.578    395
       1416.75   3.545    160
        635.13   1.590     50
        537.23   1.345    987
        530.64   1.328   1000
    

in CDCl3



liquid film