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MassMS-IW-9197 chlorodecyldimethylsilane C12H27ClSi (Mass of molecular ion: 234)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 2.4 29.0 4.9 39.0 2.0 41.0 7.6 42.0 2.2 43.0 11.5 55.0 3.8 56.0 2.4 57.0 6.7 58.0 1.0 59.0 2.8 63.0 2.2 65.0 3.6 67.0 2.0 69.0 2.4 70.0 2.2 71.0 5.5 78.0 1.1 79.0 6.2 81.0 2.5 83.0 3.4 84.0 1.5 85.0 6.0 92.0 1.6 93.0 100.0 94.0 7.8 95.0 35.3 96.0 2.7 97.0 3.8 98.0 1.0 99.0 1.0 105.0 1.2 107.0 3.6 109.0 1.3 111.0 2.2 119.0 3.0 121.0 17.4 122.0 1.7 123.0 5.7 133.0 2.5 135.0 2.8 137.0 1.1 139.0 1.1 140.0 4.5 147.0 4.0 149.0 2.6 219.0 18.2 220.0 3.0 221.0 6.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C12 H27 Cl Si 0.05 ml : 0.5 ml CDCl3 chlorodecyldimethylsilane 
Assign. Shift(ppm)
A 1.41 B 1.27 C 0.882 D 0.812 E 0.395
Hz ppm Int.562.38 1.408 35 505.98 1.267 452 359.25 0.899 83 355.83 0.891 39 352.54 0.883 265 345.46 0.865 100 332.76 0.833 70 325.07 0.814 50 316.53 0.793 80 161.50 0.405 81 158.08 0.396 1000 154.66 0.387 87
in CDCl3
liquid film
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