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MS-NW-8565 methyl vinyl sulfone C3H6O2S (Mass of molecular ion: 106)
Source Temperature: 260 °C Sample Temperature: 140 °C Reservoir, 75 eV
14.0 1.9 15.0 22.3 18.0 3.6 25.0 1.1 26.0 12.8 27.0 100.0 28.0 5.1 29.0 4.9 31.0 3.6 32.0 1.2 33.0 1.4 34.0 1.4 39.0 3.1 41.0 2.4 42.0 1.4 43.0 11.0 44.0 30.3 45.0 8.5 46.0 4.4 47.0 8.5 48.0 22.8 49.0 3.5 50.0 2.1 57.0 3.3 58.0 2.3 59.0 1.2 61.0 9.3 63.0 88.9 64.0 22.2 65.0 37.9 66.0 1.3 67.0 1.7 77.0 7.8 79.0 5.9 80.0 5.1 91.0 15.9 107.0 1.9
90 MHz in CDCl3
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1H NMR 89.56 MHz C3 H6 O2 S 0.05 ml : 0.5 ml CDCl3 methyl vinyl sulfone Assign. Shift(ppm)
A 6.771 B 6.436 C 6.116 D 2.973 J(A,B)=16.4HZ J(A,C)=9.5HZ J(B,C)=0HZ
Hz ppm Int.
623.69 6.964 48 614.19 6.858 60 607.31 6.782 110 597.75 6.675 162 581.19 6.490 243 564.81 6.307 99 556.19 6.211 238 546.69 6.105 168 266.31 2.974 1000
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