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2,4,6-三氟苯胺

产品名称 2,4,6-三氟苯胺

CAS号363-81-5

分子式C6H4F3N

分子量147.1

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  • Mass

    MS-NW-7662          
    2,4,6-trifluoroaniline
    C6H4F3N             (Mass of molecular ion:    147)
    

       Source Temperature: 260 °C
       Sample Temperature: 170 °C
       Reservoir, 75 eV
    

          28.0       2.4
          31.0       3.0
          46.0       1.0
          50.0       4.1
          51.0       4.4
          52.0       2.6
          56.0       1.9
          57.0       2.1
          63.5       1.1
          68.0       1.3
          69.0       3.6
          70.0       3.9
          73.5       5.9
          74.0       1.2
          75.0       5.2
          76.0       3.3
          77.0       1.3
          80.0       1.6
          81.0       3.5
          82.0       1.2
          93.0       1.0
          94.0       1.0
          96.0       1.6
          99.0       7.2
         100.0      24.1
         101.0       5.5
         102.0       1.0
         107.0       5.2
         108.0       1.7
         116.0       1.3
         119.0      14.2
         120.0      11.5
         126.0       4.3
         127.0      16.5
         128.0       1.9
         129.0       1.0
         146.0       7.1
         147.0     100.0
         148.0       7.2
    

90 MHz in CDCl3

400 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H4 F3 N 0.048 g : 0.5 ml CDCl3
    2,4,6-trifluoroaniline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.621 B 3.50

         Hz     ppm     Int.
    

        614.13   6.858     39
        609.44   6.805     62
        608.25   6.792     25
        605.44   6.761     69
        601.44   6.716    580
        599.69   6.696    275
        594.69   6.641    361
        592.94   6.621   1000
        591.06   6.600    301
        586.06   6.544    316
        584.38   6.526    543
        580.38   6.481     63
        576.31   6.435     66
        571.69   6.384     40
        313.19   3.497    469
    


  • 1H NMR 399.65 MHz
    C6 H4 F3 N 0.037 g : 0.5 ml CDCl3
    2,4,6-trifluoroaniline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.628 B 3.55

         Hz     ppm     Int.
    

       2657.35   6.650    624
       2656.49   6.648    366
       2655.52   6.645    278
       2653.69   6.641     56
       2650.63   6.633    297
       2649.78   6.631    371
       2648.80   6.628   1000
       2647.83   6.626    393
       2646.85   6.623    293
       2641.97   6.611    269
       2641.11   6.609    345
       2640.26   6.607    613
       1420.04   3.554    129
    

KBr disc



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