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MassMS-NW-5482 1-methyl-3-piperidinol C6H13NO (Mass of molecular ion: 115)
Source Temperature: 250 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 7.5 18.0 2.0 27.0 6.7 28.0 5.8 29.0 2.6 30.0 4.2 31.0 1.6 39.0 5.4 40.0 1.3 41.0 9.0 42.0 38.6 43.0 81.5 44.0 41.2 45.0 1.8 53.0 1.4 54.0 1.5 55.0 2.5 56.0 2.9 57.0 7.9 58.0 100.0 59.0 4.2 67.0 1.0 68.0 2.5 69.0 1.2 70.0 6.6 71.0 20.6 72.0 3.3 81.0 1.5 82.0 2.1 84.0 8.5 86.0 6.3 87.0 1.2 94.0 1.8 96.0 6.1 97.0 2.7 98.0 3.5 100.0 1.3 114.0 20.1 115.0 39.9 116.0 3.2
90 MHz in CDCl3
400 MHz in CDCl3
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1H NMR 89.56 MHz C6 H13 N O 0.04 ml : 0.5 ml CDCl3 1-methyl-3-piperidinol 
Assign. Shift(ppm)
A 3.68 B 3.77 C 2.587 D 2.41 to 2.07 E 2.252 F 1.82 to 1.30 400MHZ. : HSP-40-469
Hz ppm Int.329.81 3.683 63 229.50 2.563 31 226.44 2.529 32 205.44 2.294 37 204.31 2.282 43 201.75 2.253 1000 199.19 2.225 52 196.06 2.190 52 184.88 2.065 30 158.38 1.769 38 152.81 1.707 47 149.44 1.669 46 142.94 1.597 32
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1H NMR 399.65 MHz C6 H13 N O 0.05 ml : 0.5 ml CDCl3 1-methyl-3-piperidinol Assign. Shift(ppm)
A 4.6 B 3.729 C 2.693 D 2.488 E 2.252 F 2.13 to 2.030 G 1.81 to 1.780 J 1.550 K 1.305 90MHZ. HSP-03-345
Hz ppm Int.1498.54 3.750 40 1494.02 3.739 50 1490.23 3.729 68 1486.21 3.719 49 1481.93 3.709 40 1079.96 2.703 31 1079.35 2.701 31 1078.98 2.700 31 1078.61 2.699 31 1077.88 2.698 31 1077.27 2.696 30 1075.56 2.692 31 1072.75 2.685 32 1072.14 2.683 32 1071.78 2.682 32 996.83 2.495 31 992.92 2.485 31 992.68 2.484 31 992.19 2.483 31 991.58 2.482 31 990.97 2.480 31 900.15 2.253 1000 832.76 2.084 51 830.08 2.078 43 829.71 2.077 43 829.47 2.076 43 828.86 2.074 43 827.76 2.072 43 827.39 2.071 43 826.78 2.069 43 826.29 2.068 43 825.81 2.067 43 825.44 2.066 43 824.83 2.064 42 823.36 2.061 42 711.67 1.781 62 708.62 1.774 71 706.67 1.769 76 703.74 1.761 69 698.85 1.749 54 697.39 1.746 52 693.48 1.736 50 690.19 1.727 34 624.15 1.562 55 620.36 1.553 46 614.50 1.538 56 610.60 1.528 49 524.41 1.313 33
in CDCl3
liquid film
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