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网站主页CAS数据库列表 3554-74-3更多图谱3-羟基-N-甲基哌啶(3554-74-3)核磁图(13CNMR)

3-羟基-N-甲基哌啶

产品名称 3-羟基-N-甲基哌啶

CAS号3554-74-3

分子式C6H13NO

分子量115.17

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  • Mass

    MS-NW-5482          
    1-methyl-3-piperidinol
    C6H13NO             (Mass of molecular ion:    115)
    

       Source Temperature: 250 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          15.0       7.5
          18.0       2.0
          27.0       6.7
          28.0       5.8
          29.0       2.6
          30.0       4.2
          31.0       1.6
          39.0       5.4
          40.0       1.3
          41.0       9.0
          42.0      38.6
          43.0      81.5
          44.0      41.2
          45.0       1.8
          53.0       1.4
          54.0       1.5
          55.0       2.5
          56.0       2.9
          57.0       7.9
          58.0     100.0
          59.0       4.2
          67.0       1.0
          68.0       2.5
          69.0       1.2
          70.0       6.6
          71.0      20.6
          72.0       3.3
          81.0       1.5
          82.0       2.1
          84.0       8.5
          86.0       6.3
          87.0       1.2
          94.0       1.8
          96.0       6.1
          97.0       2.7
          98.0       3.5
         100.0       1.3
         114.0      20.1
         115.0      39.9
         116.0       3.2
    

90 MHz in CDCl3

400 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C6 H13 N O 0.04 ml : 0.5 ml CDCl3
    1-methyl-3-piperidinol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.68 B 3.77 C 2.587 D 2.41 to 2.07 E 2.252 F 1.82 to 1.30 400MHZ. : HSP-40-469

         Hz     ppm     Int.
    

        329.81   3.683     63
        229.50   2.563     31
        226.44   2.529     32
        205.44   2.294     37
        204.31   2.282     43
        201.75   2.253   1000
        199.19   2.225     52
        196.06   2.190     52
        184.88   2.065     30
        158.38   1.769     38
        152.81   1.707     47
        149.44   1.669     46
        142.94   1.597     32
    


  • 1H NMR 399.65 MHz
    C6 H13 N O 0.05 ml : 0.5 ml CDCl3
    1-methyl-3-piperidinol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.6 B 3.729 C 2.693 D 2.488 E 2.252 F 2.13 to 2.030 G 1.81 to 1.780 J 1.550 K 1.305 90MHZ. HSP-03-345

         Hz     ppm     Int.
    

       1498.54   3.750     40
       1494.02   3.739     50
       1490.23   3.729     68
       1486.21   3.719     49
       1481.93   3.709     40
       1079.96   2.703     31
       1079.35   2.701     31
       1078.98   2.700     31
       1078.61   2.699     31
       1077.88   2.698     31
       1077.27   2.696     30
       1075.56   2.692     31
       1072.75   2.685     32
       1072.14   2.683     32
       1071.78   2.682     32
        996.83   2.495     31
        992.92   2.485     31
        992.68   2.484     31
        992.19   2.483     31
        991.58   2.482     31
        990.97   2.480     31
        900.15   2.253   1000
        832.76   2.084     51
        830.08   2.078     43
        829.71   2.077     43
        829.47   2.076     43
        828.86   2.074     43
        827.76   2.072     43
        827.39   2.071     43
        826.78   2.069     43
        826.29   2.068     43
        825.81   2.067     43
        825.44   2.066     43
        824.83   2.064     42
        823.36   2.061     42
        711.67   1.781     62
        708.62   1.774     71
        706.67   1.769     76
        703.74   1.761     69
        698.85   1.749     54
        697.39   1.746     52
        693.48   1.736     50
        690.19   1.727     34
        624.15   1.562     55
        620.36   1.553     46
        614.50   1.538     56
        610.60   1.528     49
        524.41   1.313     33
    

in CDCl3



liquid film