N-叔丁基-#-苯基硝酮

产品名称 N-叔丁基-#-苯基硝酮

CAS号3376-24-7

分子式C11H15NO

分子量177.24

¹³CNMR

Mass

MS-NW-7176          
N-benzylidene-tert-butylamine N-oxide
C11H15NO            (Mass of molecular ion:    177)

   Source Temperature: 100 °C
   Sample Temperature:  80 °C
   Direct, 75 eV

      27.0       2.3
      28.0       1.0
      29.0      15.3
      39.0       5.1
      41.0      20.9
      42.0       1.1
      50.0       1.1
      51.0       2.8
      55.0       1.5
      56.0       1.7
      57.0     100.0
      58.0       4.5
      63.0       1.9
      65.0       3.7
      66.0       1.5
      77.0       4.5
      78.0       3.5
      89.0       3.1
      90.0       1.6
      92.0       1.0
      93.0       1.1
      94.0       1.8
     104.0       2.4
     120.0       3.7
     121.0      12.2
     122.0       2.2
     177.0      16.0
     178.0       2.1

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₁ H₁₅ N O	0.045 g : 0.5 ml CDCl₃
N-benzylidene-tert-butylamine N-oxide

    Assign.     Shift(ppm)

      A             8.284
      B             7.538
      C          7.46 to 7.340
      D             1.606

     Hz     ppm     Int.

    747.00   8.341     24
    743.31   8.300     29
    742.25   8.288     22
    740.31   8.267     25
    739.63   8.259     28
    737.63   8.237     29
    737.13   8.231     29
    675.13   7.539     64
    665.56   7.432     52
    664.88   7.424     40
    663.31   7.407     30
    661.63   7.388     59
    658.75   7.356     78
    143.88   1.607   1000
    141.94   1.585     62

in CDCl3

KBr disc

nujol mull

4880 A,200 M,powder

ADDUCTS WITH PHENYLAZOTRIPHENYLMETHANE

ADDUCTS WITH DI-TERT-BUTYLPEROXALATE

ADDUCTS WITH BENZOYL PEROXIDE

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N-叔丁基-#-苯基硝酮(3376-24-7)红外图谱(IR2) 相关产品图谱

N-叔丁基-#-苯基硝酮(3376-24-7)核磁图(¹³CNMR) N-叔丁基-#-苯基硝酮(3376-24-7)质谱(MS) N-叔丁基-#-苯基硝酮(3376-24-7)Raman光谱 N-叔丁基-#-苯基硝酮(3376-24-7)核磁图(¹HNMR) N-叔丁基-#-苯基硝酮(3376-24-7)ESR图谱

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