对二甲氧基苯甲醇

Mass

MS-NW-5890          
2,5-dimethoxybenzyl alcohol
C9H12O3             (Mass of molecular ion:    168)

   Source Temperature: 280 °C
   Sample Temperature: 190 °C
   Direct, 75 eV

      15.0       3.7
      18.0       1.1
      26.0       1.3
      27.0       2.8
      28.0       2.2
      29.0       2.5
      31.0       1.9
      38.0       1.7
      39.0       7.1
      40.0       1.2
      41.0       4.1
      43.0       1.7
      50.0       2.8
      51.0       5.6
      52.0       2.5
      53.0       4.5
      54.0       1.8
      55.0       6.3
      59.0       1.5
      62.0       1.7
      63.0       4.7
      64.0       3.1
      65.0      17.4
      66.0       3.1
      67.0       2.7
      69.0       1.1
      74.0       1.1
      75.0       1.0
      76.0       1.2
      76.5       2.0
      77.0      10.2
      78.0       2.7
      79.0       3.1
      81.0       3.1
      82.0       4.5
      91.0       2.4
      92.0       4.6
      93.0       8.1
      94.0       4.8
      95.0       2.1
      96.0       1.0
      97.0       2.1
     106.0       1.2
     107.0       7.8
     108.0       4.0
     109.0       5.2
     110.0      11.8
     111.0       1.1
     121.0       6.0
     122.0       1.8
     123.0       2.6
     124.0       3.8
     125.0      36.8
     126.0       3.1
     135.0      15.4
     136.0       6.0
     137.0       9.0
     138.0       2.0
     139.0      16.0
     140.0       1.6
     151.0       5.5
     152.0       5.4
     153.0      17.3
     154.0       1.6
     166.0       1.1
     167.0       2.8
     168.0     100.0
     169.0      10.3
     170.0       1.2

Assign. Shift(ppm) A 6.89 B 6.74 C 4.606 D *1 3.742 E *1 3.713 F 3.06

     Hz     ppm     Int.

   2753.42   6.890    175
   2701.29   6.760     31
   2693.85   6.741    495
   2692.38   6.737    330
   2682.74   6.713     23
   1841.31   4.608    573
   1495.61   3.743   1000
   1484.01   3.714    995
   1224.00   3.063     77