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MS-NW-5890 2,5-dimethoxybenzyl alcohol C9H12O3 (Mass of molecular ion: 168)
Source Temperature: 280 °C Sample Temperature: 190 °C Direct, 75 eV
15.0 3.7 18.0 1.1 26.0 1.3 27.0 2.8 28.0 2.2 29.0 2.5 31.0 1.9 38.0 1.7 39.0 7.1 40.0 1.2 41.0 4.1 43.0 1.7 50.0 2.8 51.0 5.6 52.0 2.5 53.0 4.5 54.0 1.8 55.0 6.3 59.0 1.5 62.0 1.7 63.0 4.7 64.0 3.1 65.0 17.4 66.0 3.1 67.0 2.7 69.0 1.1 74.0 1.1 75.0 1.0 76.0 1.2 76.5 2.0 77.0 10.2 78.0 2.7 79.0 3.1 81.0 3.1 82.0 4.5 91.0 2.4 92.0 4.6 93.0 8.1 94.0 4.8 95.0 2.1 96.0 1.0 97.0 2.1 106.0 1.2 107.0 7.8 108.0 4.0 109.0 5.2 110.0 11.8 111.0 1.1 121.0 6.0 122.0 1.8 123.0 2.6 124.0 3.8 125.0 36.8 126.0 3.1 135.0 15.4 136.0 6.0 137.0 9.0 138.0 2.0 139.0 16.0 140.0 1.6 151.0 5.5 152.0 5.4 153.0 17.3 154.0 1.6 166.0 1.1 167.0 2.8 168.0 100.0 169.0 10.3 170.0 1.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H12 O3 0.05 ml : 0.5 ml CDCl3 2,5-dimethoxybenzyl alcohol Assign. Shift(ppm)
A 6.89 B 6.74 C 4.606 D *1 3.742 E *1 3.713 F 3.06
Hz ppm Int.
2753.42 6.890 175 2701.29 6.760 31 2693.85 6.741 495 2692.38 6.737 330 2682.74 6.713 23 1841.31 4.608 573 1495.61 3.743 1000 1484.01 3.714 995 1224.00 3.063 77
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